methyl 2-<ω-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)acetyl>phenylacetate

Base Information

• Chemical Name: methyl 2-<ω-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)acetyl>phenylacetate
• CAS No.: 122775-42-2
• Molecular Formula: C₂₃H₂₇NO₅
• Molecular Weight: 397.471

Synonyms:methyl 2-<ω-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)acetyl>phenylacetate

Chemical Property of methyl 2-<ω-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)acetyl>phenylacetate

Chemical Property:

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Technology Process of methyl 2-<ω-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)acetyl>phenylacetate

There total 3 articles about methyl 2-<ω-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)acetyl>phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N,N-diethyl-3-methoxy-2-methylbenzamide (121425-20-5) → methyl 2-<ω-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)acetyl>phenylacetate (122775-42-2)

Guidance literature:

Multi-step reaction with 2 steps

1: LDA / tetrahydrofuran; hexane / Ambient temperature

2: diethyl ether

With lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane;

DOI:10.1248/cpb.37.292

Reference yield:

homophthalic anhydride (703-59-3) → methyl 2-<ω-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)acetyl>phenylacetate (122775-42-2)

Guidance literature:

Multi-step reaction with 2 steps

1: LDA / tetrahydrofuran; hexane / Ambient temperature

2: diethyl ether

With lithium diisopropyl amide; In tetrahydrofuran; diethyl ether; hexane;

DOI:10.1248/cpb.37.292

Reference yield:

diazomethane (186581-53-3,908094-01-9,334-88-3) + {2-[2-(2-Diethylcarbamoyl-6-methoxy-phenyl)-acetyl]-phenyl}-acetic acid → methyl 2-<ω-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)acetyl>phenylacetate (122775-42-2)

Guidance literature:

In diethyl ether; Yield given;

DOI:10.1248/cpb.37.292

upstream raw materials:

diazomethane

N,N-diethyl-3-methoxy-2-methylbenzamide

homophthalic anhydride

Downstream raw materials:

2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-1,3-naphthalenediol

2-(2-N,N-diethylcarbamoyl-6-methoxyphenyl)-3-hydroxy-1,4-naphthoquinone

2-(3-Hydroxy-1,4-dioxo-1,4-dihydro-naphthalen-2-yl)-3-methoxy-benzoic acid

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