C₁₄H₁₄ClN

Base Information

Chemical Name:C₁₄H₁₄ClN
CAS No.:1308305-33-0
Molecular Formula:C₁₄H₁₄ClN
Molecular Weight:231.725
Hs Code.:

Synonyms:C₁₄H₁₄ClN

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₄H₁₄ClN

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Technology Process of C₁₄H₁₄ClN

There total 3 articles about C₁₄H₁₄ClN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1246662-08-7
C₂₀H₁₇ClN₂O₄S

: 1308305-33-0
C₁₄H₁₄ClN

Guidance literature:: With potassium carbonate; thiophenol; In N,N-dimethyl-formamide; at 30 ℃; for 4h; Inert atmosphere;
DOI:10.1021/ol200958q

Reference yield:

: potassium phenyltrifluoborate

: 1308305-33-0
C₁₄H₁₄ClN

Guidance literature:: Multi-step reaction with 2 steps

1: (RhCl(C₈H₈(C₆H₄CF₃)2))2 / 1,4-dioxane; methanol / 24 h / 80 °C / Inert atmosphere

2: potassium carbonate; thiophenol / N,N-dimethyl-formamide / 4 h / 30 °C / Inert atmosphere

With (RhCl(C₈H₈(C₆H₄CF₃)2))2; potassium carbonate; thiophenol; In 1,4-dioxane; methanol; N,N-dimethyl-formamide;
DOI:10.1021/ol200958q

Reference yield:

: 98-80-6
phenylboronic acid

: 1308305-33-0
C₁₄H₁₄ClN

Guidance literature:: Multi-step reaction with 3 steps

1: potassium hydrogen difluoride / methanol; water / 0.5 h / 20 °C / Inert atmosphere

2: (RhCl(C₈H₈(C₆H₄CF₃)2))2 / 1,4-dioxane; methanol / 24 h / 80 °C / Inert atmosphere

3: potassium carbonate; thiophenol / N,N-dimethyl-formamide / 4 h / 30 °C / Inert atmosphere

With potassium hydrogen difluoride; (RhCl(C₈H₈(C₆H₄CF₃)2))2; potassium carbonate; thiophenol; In 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ol200958q