C₄₅H₆₁N₇O₅Si

Base Information

Chemical Name:C₄₅H₆₁N₇O₅Si
CAS No.:1312610-92-6
Molecular Formula:C₄₅H₆₁N₇O₅Si
Molecular Weight:808.109
Hs Code.:

C<sub>45</sub>H<sub>61</sub>N<sub>7</sub>O<sub>5</sub>Si

Synonyms:C₄₅H₆₁N₇O₅Si

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Chemical Property of C₄₅H₆₁N₇O₅Si

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Technology Process of C₄₅H₆₁N₇O₅Si

There total 7 articles about C₄₅H₆₁N₇O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 158580-57-5
methyl 4-bromo-2-nitrobenzoate

: 1312610-92-6
C₄₅H₆₁N₇O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrahydrofuran / 5 h / -40 - 20 °C / Inert atmosphere

2.1: sodium hydride / tetrahydrofuran / 1 h / 0 - 20 °C / Inert atmosphere

3.1: sodium hydroxide / methanol / 2 h / 70 °C

3.2: pH 2 - 3

4.1: oxalyl dichloride / dichloromethane / 2 h / 0 - 20 °C

5.1: dichloromethane; diethyl ether / 2 h / -10 - 20 °C / Inert atmosphere

5.2: 1 h / -10 °C

6.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

7.1: ammonium acetate / xylene / 5 h / 180 °C / Sealed tube

8.1: caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / toluene; water / 2 h / 100 °C

With oxalyl dichloride; ammonium acetate; sodium hydride; caesium carbonate; sodium hydroxide; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; toluene; xylene; 8.1: Suzuki Coupling;

Reference yield:

: 1312610-89-1
C₁₇H₂₃Br₂NO₂Si

: 1312610-92-6
C₄₅H₆₁N₇O₅Si

Guidance literature:: Multi-step reaction with 3 steps

1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 20 °C

2: ammonium acetate / xylene / 5 h / 180 °C / Sealed tube

3: caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / toluene; water / 2 h / 100 °C

With ammonium acetate; caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In water; N,N-dimethyl-formamide; toluene; xylene; 3: Suzuki Coupling;

Reference yield:

: 1312610-90-4
C₂₇H₃₉BrN₂O₆Si

: 1312610-92-6
C₄₅H₆₁N₇O₅Si

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium acetate / xylene / 5 h / 180 °C / Sealed tube

2: caesium carbonate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / toluene; water / 2 h / 100 °C

With ammonium acetate; caesium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In water; toluene; xylene; 2: Suzuki Coupling;