(S,S)-5,5''-bis-(4-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)phenyl)-[2,2':5',2'']-terthiophene

Base Information

Chemical Name:(S,S)-5,5''-bis-(4-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)phenyl)-[2,2':5',2'']-terthiophene
CAS No.:1262996-45-1
Molecular Formula:C₆₄H₇₄N₂O₁₀S₃
Molecular Weight:1127.5
Hs Code.:

Synonyms:(S,S)-5,5''-bis-(4-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)phenyl)-[2,2':5',2'']-terthiophene

Suppliers and Price of (S,S)-5,5''-bis-(4-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)phenyl)-[2,2':5',2'']-terthiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (S,S)-5,5''-bis-(4-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)phenyl)-[2,2':5',2'']-terthiophene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (S,S)-5,5''-bis-(4-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)phenyl)-[2,2':5',2'']-terthiophene

There total 6 articles about (S,S)-5,5''-bis-(4-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)phenyl)-[2,2':5',2'']-terthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1046451-11-9
(S)-4-iodo-1-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)benzene

: 1259016-23-3
2,2'-([2,2':5',2''-terthiophene]-5,5''-diyl)bis(4,4,5,5-tetramethyl-1,3,2-dioxaborolane)

: 1262996-45-1
(S,S)-5,5''-bis-(4-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)phenyl)-[2,2':5',2'']-terthiophene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; silver(l) oxide; In 1,4-dioxane; at 70 ℃; Inert atmosphere;
DOI:10.1016/j.tet.2010.11.004

Reference yield:

: 1081-34-1
2,2':5',2''-terthiophene

: 1262996-45-1
(S,S)-5,5''-bis-(4-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)phenyl)-[2,2':5',2'']-terthiophene

Guidance literature:: Multi-step reaction with 2 steps

1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 4,4'-di-tert-butyl-2,2'-bipyridine / octane / 12 h / 90 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; silver(l) oxide / 1,4-dioxane / 70 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(1,5-cyclooctadiene)diiridium(I) dichloride; sodium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine; silver(l) oxide; In 1,4-dioxane; octane; 2: Suzuki-Miyaura coupling;
DOI:10.1016/j.tet.2010.11.004

Reference yield:

: 479719-88-5
2-([2,2'-bithiophen]-5-yl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1262996-45-1
(S,S)-5,5''-bis-(4-(6-(2-tert-butoxycarbonylamino-3-phenylpropanoyloxy)hexyloxy)phenyl)-[2,2':5',2'']-terthiophene

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate / ethanol; water; toluene / 95 °C / Inert atmosphere

2: bis(1,5-cyclooctadiene)diiridium(I) dichloride; 4,4'-di-tert-butyl-2,2'-bipyridine / octane / 12 h / 90 °C / Inert atmosphere

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; sodium carbonate; silver(l) oxide / 1,4-dioxane / 70 °C / Inert atmosphere

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; bis(1,5-cyclooctadiene)diiridium(I) dichloride; sodium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine; silver(l) oxide; In 1,4-dioxane; octane; ethanol; water; toluene; 1: Suzuki-Miyaura coupling / 3: Suzuki-Miyaura coupling;
DOI:10.1016/j.tet.2010.11.004