2-(S)-[2-(S)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)-propionylamino]-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester

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Chemical Name:2-(S)-[2-(S)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)-propionylamino]-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester
CAS No.:1192849-64-1
Molecular Formula:C₃₂H₃₇IN₂O₈
Molecular Weight:704.559
Hs Code.:

Synonyms:2-(S)-[2-(S)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)-propionylamino]-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester

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Chemical Property of 2-(S)-[2-(S)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)-propionylamino]-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester

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Technology Process of 2-(S)-[2-(S)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)-propionylamino]-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester

There total 1 articles about 2-(S)-[2-(S)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)-propionylamino]-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 53267-93-9
O-methyl-N-tert-butoxycarbonyl-L-tyrosine

: 327621-03-4
2-(S)-tert-butoxycarbonylamino-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester

: 1192849-64-1
2-(S)-[2-(S)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)-propionylamino]-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester

Guidance literature:: 2-(S)-tert-butoxycarbonylamino-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester; With acetyl chloride; In tetrahydrofuran; methanol; at 20 ℃;

O-methyl-N-tert-butoxycarbonyl-L-tyrosine; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃;
DOI:10.1021/jo9018792

Reference yield: 80.0%

: 1192849-64-1
2-(S)-[2-(S)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)-propionylamino]-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester

: 190579-73-8
2-benzyloxycarbonylamino-3-iodo-propionic acid tert-butyl ester

: 1192849-65-2
3-{4-[5-(2-(S)-benzyloxycarbonylamino-2-tert-butoxycarbonylethyl)-2-methoxyphenoxy]phenyl}-2-(S)-[2-(S)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)propionylamino]propionic acid methyl ester

Guidance literature:: 2-benzyloxycarbonylamino-3-iodo-propionic acid tert-butyl ester; With chloro-trimethyl-silane; zinc; In N,N-dimethyl-formamide; Inert atmosphere; Cooling with ice;

2-(S)-[2-(S)-tert-butoxycarbonylamino-3-(4-methoxyphenyl)-propionylamino]-3-[4-(5-iodo-2-methoxyphenoxy)phenyl]propionic acid methyl ester; With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tris-(o-tolyl)phosphine; In N,N-dimethyl-formamide; at 20 - 50 ℃; Inert atmosphere;
DOI:10.1021/jo9018792