<4-13C>Benzylbromid

Base Information

Chemical Name:<4-13C>Benzylbromid
CAS No.:87295-46-3
Molecular Formula:C₇H₇Br
Molecular Weight:172.026
Hs Code.:

Synonyms:<4-13C>Benzylbromid

Suppliers and Price of <4-13C>Benzylbromid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <4-13C>Benzylbromid

Chemical Property:

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Technology Process of <4-13C>Benzylbromid

There total 8 articles about <4-13C>Benzylbromid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 78218-02-7
<4-13C>toluene

: 87295-46-3
<4-13C>Benzylbromid

Guidance literature:: With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); In tetrachloromethane; pentane; at 85 ℃;

Reference yield:

: 87295-54-3
<3-13C>Pentan-1,5-diol

: 87295-46-3
<4-13C>Benzylbromid

Guidance literature:: Multi-step reaction with 5 steps

1: 4.2 g / conc. HBr / 8 h / 100 - 105 °C

2: 1.) Mg, I₂ / 1.) THF, 2h, r.t., 2.) THF, 20 h

3: 95 percent / I₂ / tetrahydrofuran / 0.75 h / 150 °C

4: 96 percent Chromat_. / 10 percent Pd/C / pentane / 400 °C

5: 64 percent / NBS, azobis(isobutyronitrile) / CCl₄; pentane / 85 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); hydrogen bromide; iodine; magnesium; palladium on activated charcoal; In tetrahydrofuran; tetrachloromethane; pentane;

Reference yield:

: 87295-44-1
<4-13C>-1-Methylcyclohexanol

: 87295-46-3
<4-13C>Benzylbromid

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / I₂ / tetrahydrofuran / 0.75 h / 150 °C

2: 96 percent Chromat_. / 10 percent Pd/C / pentane / 400 °C

3: 64 percent / NBS, azobis(isobutyronitrile) / CCl₄; pentane / 85 °C

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); iodine; palladium on activated charcoal; In tetrahydrofuran; tetrachloromethane; pentane;