3-(2',4'-Dimethylphenyl)-6-carbethoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid

Base Information

• Chemical Name: 3-(2',4'-Dimethylphenyl)-6-carbethoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid
• CAS No.: 77239-65-7
• Molecular Formula: C₁₈H₂₀O₅
• Molecular Weight: 316.354

Synonyms:3-(2',4'-Dimethylphenyl)-6-carbethoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid

Chemical Property of 3-(2',4'-Dimethylphenyl)-6-carbethoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid

Chemical Property:

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Technology Process of 3-(2',4'-Dimethylphenyl)-6-carbethoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid

There total 1 articles about 3-(2',4'-Dimethylphenyl)-6-carbethoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

ethyl acetoacetate (141-97-9) + 2-[2-(2,4-Dimethyl-phenyl)-2-oxo-ethyl]-3-ethoxycarbonyl-succinic acid 4-ethyl ester (77239-53-3) → 3-(2',4'-Dimethylphenyl)-6-carbethoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid (77239-65-7)

Guidance literature:

With sodium methylate; at 170 ℃; for 10h;

Reference yield: 85.0%

3-(2',4'-Dimethylphenyl)-6-carbethoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid (77239-65-7) → 3-(2,4-Dimethyl-phenyl)-5-oxo-cyclohex-3-enecarboxylic acid (77239-69-1)

Guidance literature:

With potassium hydroxide; In ethanol; for 8h;

Reference yield: 80.0%

3-(2',4'-Dimethylphenyl)-6-carbethoxy-5-oxo-cyclohex-3-ene-1-carboxylic acid (77239-65-7) → 3-(2,4-Dimethyl-phenyl)-5-[(E)-hydroxyimino]-cyclohex-3-enecarboxylic acid (77239-75-9)

Guidance literature:

With hydroxylamine; sodium acetate; In ethanol; for 8h; Heating;

upstream raw materials:

ethyl acetoacetate

2-[2-(2,4-Dimethyl-phenyl)-2-oxo-ethyl]-3-ethoxycarbonyl-succinic acid 4-ethyl ester

Downstream raw materials:

3-(2,4-Dimethyl-phenyl)-5-oxo-cyclohex-3-enecarboxylic acid

3-(2,4-Dimethyl-phenyl)-5-[(E)-hydroxyimino]-cyclohex-3-enecarboxylic acid

5-(2,4-Dimethyl-phenyl)-3-hydrazono-cyclohex-4-ene-1,2-dicarboxylic acid 2-ethyl ester

6-(2',5'-Dimethylphenyl)-3(H)-oxo-2-phenyl-3,3a,4,5-tetrahydroindazole-4-carboxylic acid

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