(2S)-5-amino-N-benzyl-2-[(S)-5-benzyl-2,4-dioxo-3-phenylimidazolidin-1-yl]pentanamide trifluoroacetate

Base Information

• Chemical Name: (2S)-5-amino-N-benzyl-2-[(S)-5-benzyl-2,4-dioxo-3-phenylimidazolidin-1-yl]pentanamide trifluoroacetate
• CAS No.: 1607465-92-8
• Molecular Formula: C₂HF₃O₂*C₂₈H₃₀N₄O₃
• Molecular Weight: 584.595

Synonyms:(2S)-5-amino-N-benzyl-2-[(S)-5-benzyl-2,4-dioxo-3-phenylimidazolidin-1-yl]pentanamide trifluoroacetate

Chemical Property of (2S)-5-amino-N-benzyl-2-[(S)-5-benzyl-2,4-dioxo-3-phenylimidazolidin-1-yl]pentanamide trifluoroacetate

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Technology Process of (2S)-5-amino-N-benzyl-2-[(S)-5-benzyl-2,4-dioxo-3-phenylimidazolidin-1-yl]pentanamide trifluoroacetate

There total 3 articles about (2S)-5-amino-N-benzyl-2-[(S)-5-benzyl-2,4-dioxo-3-phenylimidazolidin-1-yl]pentanamide trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

C33H39N5O4 (1419178-27-0) → (2S)-5-amino-N-benzyl-2-[(S)-5-benzyl-2,4-dioxo-3-phenylimidazolidin-1-yl]pentanamide trifluoroacetate (1607465-92-8)

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h; Reagent/catalyst; Temperature; Time;

DOI:10.1016/j.tet.2014.03.082

Reference yield: 55.0%

C33H39N5O4 (1419178-27-0) → (2S)-5-amino-N-benzyl-2-[(S)-5-benzyl-2,4-dioxo-3-phenylimidazolidin-1-yl]pentanamide trifluoroacetate (1607465-92-8) + C28H31N5O2 (1607465-83-7)

Guidance literature:

With hydrogenchloride; In ethyl acetate; at 20 ℃; for 0.5h;

DOI:10.1016/j.tet.2014.03.082

Reference yield: 28.0%

C33H39N5O4 → (2S)-5-amino-N-benzyl-2-[(S)-5-benzyl-2,4-dioxo-3-phenylimidazolidin-1-yl]pentanamide trifluoroacetate (1607465-92-8) + (2S)-5-amino-N-benzyl-2-[(R)-5-benzyl-2,4-dioxo-3-phenylimidazolidin-1-yl]pentanamide trifluoroacetate

Guidance literature:

With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 24h; Reagent/catalyst; Temperature; Time; Overall yield = 96 %;

DOI:10.1016/j.tet.2014.03.082

upstream raw materials:

C₃₃H₃₉N₅O₄

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