C₂₃H₂₈OS₂

Base Information

Chemical Name:C₂₃H₂₈OS₂
CAS No.:1454583-26-6
Molecular Formula:C₂₃H₂₈OS₂
Molecular Weight:384.607
Hs Code.:

C<sub>23</sub>H<sub>28</sub>OS<sub>2</sub>

Synonyms:C₂₃H₂₈OS₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₃H₂₈OS₂

Chemical Property:

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Technology Process of C₂₃H₂₈OS₂

There total 1 articles about C₂₃H₂₈OS₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 65016-62-8,104934-51-2
3-octylthiophene

: 1454583-26-6
C₂₃H₂₈OS₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-Bromosuccinimide / tetrahydrofuran / 15 h / 25 °C

2.1: magnesium / tetrahydrofuran / 0.5 h / Reflux

2.2: 15 h / Reflux

With N-Bromosuccinimide; magnesium; In tetrahydrofuran; 2.2: |Kumada Cross-Coupling;
DOI:10.1039/c3sc50664a

Reference yield:

: 1454583-26-6
C₂₃H₂₈OS₂

: 1454583-85-7
C₅₀H₆₂O₆S₄

Guidance literature:: Multi-step reaction with 6 steps

1: boron tribromide / dichloromethane / 24 h / -78 - 25 °C

2: potassium carbonate / acetonitrile / 6 h / Reflux

3: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 25 °C

4: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / 24 h / 25 °C

5: n-butyllithium; copper dichloride / tetrahydrofuran / 15 h / -60 °C / Reflux

6: hydrogenchloride / water; methanol / 24 h / 25 °C

With hydrogenchloride; osmium(VIII) oxide; n-butyllithium; pyridinium p-toluenesulfonate; boron tribromide; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; copper dichloride; In tetrahydrofuran; methanol; dichloromethane; water; acetone; acetonitrile;
DOI:10.1039/c3sc50664a

Reference yield:

: 1454583-26-6
C₂₃H₂₈OS₂

: 1454583-61-9
C₂₈H₃₆O₃S₂

Guidance literature:: Multi-step reaction with 4 steps

1: boron tribromide / dichloromethane / 24 h / -78 - 25 °C

2: potassium carbonate / acetonitrile / 6 h / Reflux

3: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone / 25 °C

4: pyridinium p-toluenesulfonate; toluene-4-sulfonic acid / 24 h / 25 °C

With osmium(VIII) oxide; pyridinium p-toluenesulfonate; boron tribromide; potassium carbonate; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; In dichloromethane; water; acetone; acetonitrile;
DOI:10.1039/c3sc50664a