C₂₈H₃₉NO₅Si

Base Information

Chemical Name:C₂₈H₃₉NO₅Si
CAS No.:1586799-34-9
Molecular Formula:C₂₈H₃₉NO₅Si
Molecular Weight:497.707
Hs Code.:

C<sub>28</sub>H<sub>39</sub>NO<sub>5</sub>Si

Synonyms:C₂₈H₃₉NO₅Si

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Chemical Property of C₂₈H₃₉NO₅Si

Chemical Property:

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Technology Process of C₂₈H₃₉NO₅Si

There total 15 articles about C₂₈H₃₉NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1543007-32-4
C₂₈H₃₉NO₄Si

: 1586799-34-9
C₂₈H₃₉NO₅Si

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; In water; tert-butyl alcohol; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tet.2013.12.078

Reference yield:

: 1543006-73-0
(2R,3S)-2-allyl-5-(benzyloxy)pentane-1,3-diol

: 1586799-34-9
C₂₈H₃₉NO₅Si

Guidance literature:: Multi-step reaction with 14 steps

1.1: camphor-10-sulfonic acid / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; toluene / 4 h / 20 °C / Inert atmosphere

3.1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.75 h / 0 °C / pH Ca_. 7 / Inert atmosphere

4.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

5.1: triethylamine; dmap / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

6.1: sodium azide / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

7.1: acetic acid; water / 3 h / 100 °C / Inert atmosphere

8.1: triethylamine; dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

9.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

10.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

10.2: 36 h / Inert atmosphere; Reflux

11.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

12.1: palladium 10% on activated carbon; hydrogen / methanol / 6 h

13.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

13.2: 1 h / -78 - 0 °C / Inert atmosphere

14.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

With dmap; sodium chlorite; sodium tetrahydroborate; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; sodium azide; 2-methyl-but-2-ene; oxalyl dichloride; palladium 10% on activated carbon; camphor-10-sulfonic acid; water; hydrogen; acetic acid; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.12.078

Reference yield:

: 1543006-77-4
(4S,5R)-5-allyl-4-(2-(benzyloxy)ethyl)-2,2-dimethyl-1,3-dioxane

: 1586799-34-9
C₂₈H₃₉NO₅Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / water; acetone; toluene / 4 h / 20 °C / Inert atmosphere

2.1: sodium periodate / tetrahydrofuran; aq. phosphate buffer / 0.75 h / 0 °C / pH Ca_. 7 / Inert atmosphere

3.1: sodium tetrahydroborate / methanol / 1 h / 0 °C / Inert atmosphere

4.1: triethylamine; dmap / N,N-dimethyl-formamide / 2 h / 20 °C / Inert atmosphere

5.1: sodium azide / N,N-dimethyl-formamide / 6 h / 80 °C / Inert atmosphere

6.1: acetic acid; water / 3 h / 100 °C / Inert atmosphere

7.1: triethylamine; dmap / dichloromethane / 5 h / 20 °C / Inert atmosphere

8.1: triethylamine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

9.1: triphenylphosphine / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

9.2: 36 h / Inert atmosphere; Reflux

10.1: tetrahydrofuran / 12 h / 20 °C / Inert atmosphere

11.1: palladium 10% on activated carbon; hydrogen / methanol / 6 h

12.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

12.2: 1 h / -78 - 0 °C / Inert atmosphere

13.1: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogenphosphate / water; tert-butyl alcohol / 3 h / 20 °C / Inert atmosphere

With dmap; sodium chlorite; sodium tetrahydroborate; sodium periodate; sodium dihydrogenphosphate; osmium(VIII) oxide; sodium azide; 2-methyl-but-2-ene; oxalyl dichloride; palladium 10% on activated carbon; water; hydrogen; acetic acid; dimethyl sulfoxide; 4-methylmorpholine N-oxide; triethylamine; triphenylphosphine; In tetrahydrofuran; methanol; aq. phosphate buffer; dichloromethane; water; N,N-dimethyl-formamide; acetone; toluene; tert-butyl alcohol;
DOI:10.1016/j.tet.2013.12.078