2-benzoyl naphtho<1,2-d>oxazole

Base Information

• Chemical Name: 2-benzoyl naphtho<1,2-d>oxazole
• CAS No.: 25674-67-3
• Molecular Formula: C₁₈H₁₁NO₂
• Molecular Weight: 273.291

Synonyms:2-benzoyl naphtho<1,2-d>oxazole

Chemical Property of 2-benzoyl naphtho<1,2-d>oxazole

Chemical Property:

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Technology Process of 2-benzoyl naphtho<1,2-d>oxazole

There total 4 articles about 2-benzoyl naphtho<1,2-d>oxazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

N-phenacylpyridinium bromide (16883-69-5) + 1-Nitroso-2-naphthol (131-91-9) → 2-benzoyl naphtho<1,2-d>oxazole (25674-67-3)

Guidance literature:

With sodium hydroxide; In ethanol; at -10 - 20 ℃; for 2.5h;

DOI:10.1021/jo3022956

Reference yield: 50.0%

1-Nitroso-2-naphthol (131-91-9) + trans-1-cyclohexyl-2-phenyl-3-benzoylaziridine (2211-61-2) → 2-benzoyl naphtho<1,2-d>oxazole (25674-67-3) + 2-phenylnaphtho[1,2-d]oxazole (3574-02-5)

Guidance literature:

In neat (no solvent); for 0.2h; Irradiation;

DOI:10.1016/0040-4039(96)00795-2

Reference yield:

[1-cyclohexyl-3-(4-nitro-phenyl)-aziridin-2-yl]-phenyl-methanone (94862-23-4) + 1-Nitroso-2-naphthol (131-91-9) → 2-benzoyl naphtho<1,2-d>oxazole (25674-67-3)

Guidance literature:

In benzene; Heating;

DOI:10.1139/v70-371

upstream raw materials:

[1-cyclohexyl-3-(4-nitro-phenyl)-aziridin-2-yl]-phenyl-methanone

1-Nitroso-2-naphthol

N-phenacylpyridinium bromide

trans-1-cyclohexyl-2-phenyl-3-benzoylaziridine

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