cis-9,10-decalinediol allyl 2-triphenylmethoxyethyl ether

Base Information

Chemical Name:cis-9,10-decalinediol allyl 2-triphenylmethoxyethyl ether
CAS No.:259866-65-4
Molecular Formula:C₃₄H₄₀O₃
Molecular Weight:496.69
Hs Code.:

Synonyms:cis-9,10-decalinediol allyl 2-triphenylmethoxyethyl ether

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Chemical Property of cis-9,10-decalinediol allyl 2-triphenylmethoxyethyl ether

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Technology Process of cis-9,10-decalinediol allyl 2-triphenylmethoxyethyl ether

There total 6 articles about cis-9,10-decalinediol allyl 2-triphenylmethoxyethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 259866-64-3
cis-9,10-decalinediol mono(2-triphenylmethoxyethyl) ether

: 106-95-6
allyl bromide

: 259866-65-4
cis-9,10-decalinediol allyl 2-triphenylmethoxyethyl ether

Guidance literature:: cis-9,10-decalinediol mono(2-triphenylmethoxyethyl) ether; With sodium hydride; In tetrahydrofuran; for 2h; Heating;

allyl bromide; In tetrahydrofuran; for 16h; Further stages.; Heating;
DOI:10.1021/ac025713+

Reference yield:

: 259866-63-2
cis-9,10-decalinediol mono(2-hydroxyethyl) ether

: 259866-65-4
cis-9,10-decalinediol allyl 2-triphenylmethoxyethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: 82 percent / pyridine / 16 h / 60 °C

2.1: NaH / tetrahydrofuran / 2 h / Heating

2.2: 94 percent / tetrahydrofuran / 16 h / Heating

With pyridine; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ac025713+

Reference yield:

: 259866-61-0
(8a-hydroxy-octahydro-naphthalen-4a-yloxy)-acetic acid

: 259866-65-4
cis-9,10-decalinediol allyl 2-triphenylmethoxyethyl ether

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1.21 g / p-toluenesulfonic acid; 3 Angstroem molecular sieves / benzene / 15 h / Heating

2.1: 100 percent / LiAlH₄ / tetrahydrofuran / 3 h / Heating

3.1: 82 percent / pyridine / 16 h / 60 °C

4.1: NaH / tetrahydrofuran / 2 h / Heating

4.2: 94 percent / tetrahydrofuran / 16 h / Heating

With pyridine; lithium aluminium tetrahydride; 3 A molecular sieve; sodium hydride; toluene-4-sulfonic acid; In tetrahydrofuran; benzene;
DOI:10.1021/ac025713+