N,N'-diphenyloxalodihydrazonyl diazide

Base Information

• Chemical Name: N,N'-diphenyloxalodihydrazonyl diazide
• CAS No.: 149452-07-3
• Molecular Formula: C₁₄H₁₂N₁₀
• Molecular Weight: 320.316

Synonyms:N,N'-diphenyloxalodihydrazonyl diazide

Chemical Property of N,N'-diphenyloxalodihydrazonyl diazide

Chemical Property:

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Technology Process of N,N'-diphenyloxalodihydrazonyl diazide

There total 1 articles about N,N'-diphenyloxalodihydrazonyl diazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

N,N'-diphenylethane(bis-hydrazonoyl dichloride) (31805-14-8) → N,N'-diphenyloxalodihydrazonyl diazide (149452-07-3)

Guidance literature:

With sodium azide; In water; N,N-dimethyl-formamide; for 10h; Ambient temperature;

DOI:10.1016/S0040-4020(01)86352-3

Reference yield: 75.0%

triphenylphosphine (603-35-0) + N,N'-diphenyloxalodihydrazonyl diazide (149452-07-3) → 1,2-bis(triphenylphosphinimino) glyoxal bis(phenylhydrazone) (149452-19-7)

Guidance literature:

In benzene; for 3h; Heating;

DOI:10.1016/S0040-4020(01)86352-3

Reference yield: 72.0%

N,N'-diphenyloxalodihydrazonyl diazide (149452-07-3) → N1,N1'-diphenyloxaldiamidrazone (3449-06-7)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; for 4h; Heating;

DOI:10.1016/S0040-4020(01)86352-3

upstream raw materials:

N,N'-diphenylethane(bis-hydrazonoyl dichloride)

Downstream raw materials:

1,2-bis(triphenylphosphinimino) glyoxal bis(phenylhydrazone)

N¹,N^1'-diphenyloxaldiamidrazone

1,5,1',5'-tetraphenyl-1H,1'H-[3,3']bi[1,2,4]triazolyl

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