2-N-tert-butoxycarbonyl-amino-isobutyric acid [3-methyl-4-(3-oxo-morpholin-4-yl)phenyl]amide

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Chemical Name:2-N-tert-butoxycarbonyl-amino-isobutyric acid [3-methyl-4-(3-oxo-morpholin-4-yl)phenyl]amide
CAS No.:869785-63-7
Molecular Formula:C₂₀H₂₉N₃O₅
Molecular Weight:391.467
Hs Code.:

Synonyms:2-N-tert-butoxycarbonyl-amino-isobutyric acid [3-methyl-4-(3-oxo-morpholin-4-yl)phenyl]amide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-N-tert-butoxycarbonyl-amino-isobutyric acid [3-methyl-4-(3-oxo-morpholin-4-yl)phenyl]amide

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Technology Process of 2-N-tert-butoxycarbonyl-amino-isobutyric acid [3-methyl-4-(3-oxo-morpholin-4-yl)phenyl]amide

There total 2 articles about 2-N-tert-butoxycarbonyl-amino-isobutyric acid [3-methyl-4-(3-oxo-morpholin-4-yl)phenyl]amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 30992-29-1
Boc-Aib-OH

: 482308-10-1
4-(4-amino-2-methylphenyl)morpholin-3-one

: 869785-63-7
2-N-tert-butoxycarbonyl-amino-isobutyric acid [3-methyl-4-(3-oxo-morpholin-4-yl)phenyl]amide

Guidance literature:: With 4-methyl-morpholine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; at 30 ℃; for 5.33333h;

Reference yield: 38.0%

: 482308-10-1
4-(4-amino-2-methylphenyl)morpholin-3-one

: 869785-63-7
2-N-tert-butoxycarbonyl-amino-isobutyric acid [3-methyl-4-(3-oxo-morpholin-4-yl)phenyl]amide

Guidance literature:: Boc-Aib-OH; With 4-methyl-morpholine; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 2h;

4-(4-amino-2-methylphenyl)morpholin-3-one; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 16h;