5-(2-methoxybenzamido)-6-(piperidin-1-yl)-2-(thiophen-2-yl)-1H-benzo[d]imidazole

Base Information

Chemical Name:5-(2-methoxybenzamido)-6-(piperidin-1-yl)-2-(thiophen-2-yl)-1H-benzo[d]imidazole
CAS No.:1434143-09-5
Molecular Formula:C₂₄H₂₄N₄O₂S
Molecular Weight:432.546
Hs Code.:

Synonyms:5-(2-methoxybenzamido)-6-(piperidin-1-yl)-2-(thiophen-2-yl)-1H-benzo[d]imidazole

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Chemical Property of 5-(2-methoxybenzamido)-6-(piperidin-1-yl)-2-(thiophen-2-yl)-1H-benzo[d]imidazole

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Technology Process of 5-(2-methoxybenzamido)-6-(piperidin-1-yl)-2-(thiophen-2-yl)-1H-benzo[d]imidazole

There total 6 articles about 5-(2-methoxybenzamido)-6-(piperidin-1-yl)-2-(thiophen-2-yl)-1H-benzo[d]imidazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 1434143-03-9
5-amino-6-(piperidin-1-yl)-2-(thiophen-2-yl)-1H-benzo[d]imidazole

: 21615-34-9
2-Methoxybenzoyl chloride

: 1434143-09-5
5-(2-methoxybenzamido)-6-(piperidin-1-yl)-2-(thiophen-2-yl)-1H-benzo[d]imidazole

Guidance literature:: In dichloromethane; at 20 ℃;
DOI:10.1016/j.bmc.2013.02.059

Reference yield:

: C₁₆H₂₀N₄OS

: 1434143-09-5
5-(2-methoxybenzamido)-6-(piperidin-1-yl)-2-(thiophen-2-yl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol; water; 1,4-dioxane / 6 h / Reflux

2: dichloromethane / 20 °C

With hydrogenchloride; In 1,4-dioxane; ethanol; dichloromethane; water;
DOI:10.1016/j.bmc.2013.02.059

Reference yield:

: 1434143-00-6
2,4-dinitro-1-(2-thiophenyl)carboxamido-5-(piperidin-1-yl)benzene

: 1434143-09-5
5-(2-methoxybenzamido)-6-(piperidin-1-yl)-2-(thiophen-2-yl)-1H-benzo[d]imidazole

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; ammonium formate / ethanol; 1,4-dioxane / 1 h / 20 °C

2: hydrogenchloride / ethanol; water; 1,4-dioxane / 6 h / Reflux

3: dichloromethane / 20 °C

With hydrogenchloride; palladium 10% on activated carbon; ammonium formate; In 1,4-dioxane; ethanol; dichloromethane; water;
DOI:10.1016/j.bmc.2013.02.059