14,15-dihydromanool

Base Information

Chemical Name:14,15-dihydromanool
CAS No.:40768-86-3
Molecular Formula:C₂₀H₃₆O
Molecular Weight:292.505
Hs Code.:

Synonyms:14,15-dihydromanool

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Chemical Property of 14,15-dihydromanool

Chemical Property:

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Technology Process of 14,15-dihydromanool

There total 2 articles about 14,15-dihydromanool which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 596-85-0
manool

: 40768-86-3
(4aS)-5.5.8at-trimethyl-1t-((S)-3-hydroxy-3-methyl-pentyl)-(4arH)-2-methylene-decalin

Guidance literature:: With hydrogen; platinum(IV) oxide; In methanol; Ambient temperature;
DOI:10.1016/S0040-4039(97)01004-6

Reference yield:

: 596-85-0
epimanool

: 40768-86-3
14,15-dihydromanool

Guidance literature:: With potassium carbonate; toluene-4-sulfonic acid hydrazide; In 2-methoxy-ethanol; at 95 - 100 ℃; for 45h;
DOI:10.1021/jo00320a027

Reference yield:

: 40768-86-3
14,15-dihydromanool

: 596-85-0
epimanool

Guidance literature:: Multi-step reaction with 2 steps

1: 0.35 g / POCl₃ / pyridine / 24 h / 0 °C

2: 1.) oxygen, rose bengal, 2.) triethyl phosphite / 1.) CH₂Cl₂, CH₃OH, irradiation, 60 min

With oxygen; rose bengal; triethyl phosphite; trichlorophosphate; In pyridine;
DOI:10.1021/jo00320a027