N,N'-bis<6-hexanoyl>-1,6-hexanediamine

Base Information

Chemical Name:N,N'-bis<6-hexanoyl>-1,6-hexanediamine
CAS No.:156272-97-8
Molecular Formula:C₅₆H₆₆N₄O₆
Molecular Weight:891.163
Hs Code.:

N,N'-bis<6-<N-(2-naphthylmethyl)-N-carbobenzoxyamino>hexanoyl>-1,6-hexanediamine

Synonyms:N,N'-bis<6-hexanoyl>-1,6-hexanediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-bis<6-hexanoyl>-1,6-hexanediamine

Chemical Property:

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Technology Process of N,N'-bis<6-hexanoyl>-1,6-hexanediamine

There total 6 articles about N,N'-bis<6-hexanoyl>-1,6-hexanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 124-09-4
1,6-Hexanediamine

: 156272-90-1
6-hexanoic acid N-hydroxysuccinimide ester

: 156272-97-8
N,N'-bis<6-hexanoyl>-1,6-hexanediamine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 18h;
DOI:10.1021/jm00040a018

Reference yield:

: 66-99-9
β-naphthaldehyde

: 156272-97-8
N,N'-bis<6-hexanoyl>-1,6-hexanediamine

Guidance literature:: Multi-step reaction with 5 steps

1: toluene / 18 h / Heating

2: sodium borohydride / ethanol / 8 h

3: 97 percent / NaHCO₃ / H₂O / 6 h / 0 °C

4: 70 percent / dicyclohexylcarbodiimide / CH₂Cl₂

5: 79 percent / DIEA / CH₂Cl₂ / 18 h

With sodium tetrahydroborate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water; toluene;
DOI:10.1021/jm00040a018

Reference yield:

: 6-{[1-Naphthalen-2-yl-meth-(E)-ylidene]-amino}-hexanoic acid

: 156272-97-8
N,N'-bis<6-hexanoyl>-1,6-hexanediamine

Guidance literature:: Multi-step reaction with 4 steps

1: sodium borohydride / ethanol / 8 h

2: 97 percent / NaHCO₃ / H₂O / 6 h / 0 °C

3: 70 percent / dicyclohexylcarbodiimide / CH₂Cl₂

4: 79 percent / DIEA / CH₂Cl₂ / 18 h

With sodium tetrahydroborate; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; dicyclohexyl-carbodiimide; In ethanol; dichloromethane; water;
DOI:10.1021/jm00040a018