3,3',3,3'-(5,5'-(9H-fluorene-9,9-diyl)bis(2-(oxirane-2-ylmethoxy)benzene-5,3,1-triyl))(tetrakis propane-3,1-diyl)tetrakis(triethoxysilane)

Base Information

Chemical Name:3,3',3,3'-(5,5'-(9H-fluorene-9,9-diyl)bis(2-(oxirane-2-ylmethoxy)benzene-5,3,1-triyl))(tetrakis propane-3,1-diyl)tetrakis(triethoxysilane)
CAS No.:1422984-43-7
Molecular Formula:C₆₇H₁₀₆O₁₆Si₄
Molecular Weight:1279.91
Hs Code.:

Synonyms:3,3',3,3'-(5,5'-(9H-fluorene-9,9-diyl)bis(2-(oxirane-2-ylmethoxy)benzene-5,3,1-triyl))(tetrakis propane-3,1-diyl)tetrakis(triethoxysilane)

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Chemical Property of 3,3',3,3'-(5,5'-(9H-fluorene-9,9-diyl)bis(2-(oxirane-2-ylmethoxy)benzene-5,3,1-triyl))(tetrakis propane-3,1-diyl)tetrakis(triethoxysilane)

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Technology Process of 3,3',3,3'-(5,5'-(9H-fluorene-9,9-diyl)bis(2-(oxirane-2-ylmethoxy)benzene-5,3,1-triyl))(tetrakis propane-3,1-diyl)tetrakis(triethoxysilane)

There total 6 articles about 3,3',3,3'-(5,5'-(9H-fluorene-9,9-diyl)bis(2-(oxirane-2-ylmethoxy)benzene-5,3,1-triyl))(tetrakis propane-3,1-diyl)tetrakis(triethoxysilane) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 998-30-1
Triethoxysilane

: 1422984-41-5
2,2'-(4,4'-(9H-fluorene-9,9-diyl)bis(2,6-diallyl-4,1-phenylene)bis(oxy)bis(methylene))dioxirane

: 1422984-43-7
3,3',3,3'-(5,5'-(9H-fluorene-9,9-diyl)bis(2-(oxirane-2-ylmethoxy)benzene-5,3,1-triyl))(tetrakis propane-3,1-diyl)tetrakis(triethoxysilane)

Guidance literature:: With platinum(IV) oxide; In toluene; at 85 ℃; for 24h; Inert atmosphere;

Reference yield:

: 3236-71-3
9,9-bis(4-hydroxyphenyl)fluorene

: 1422984-43-7
3,3',3,3'-(5,5'-(9H-fluorene-9,9-diyl)bis(2-(oxirane-2-ylmethoxy)benzene-5,3,1-triyl))(tetrakis propane-3,1-diyl)tetrakis(triethoxysilane)

Guidance literature:: Multi-step reaction with 6 steps

1: potassium carbonate / acetone / 80 °C

2: 1,2-dichloro-benzene / 96 h / 20 - 190 °C

3: potassium carbonate / acetone / 80 °C

4: 1,2-dichloro-benzene / 8 h / 20 - 190 °C

5: potassium carbonate / acetonitrile / 20 - 80 °C

6: platinum(IV) oxide / toluene / 24 h / 85 °C / Inert atmosphere

With platinum(IV) oxide; potassium carbonate; In 1,2-dichloro-benzene; acetone; toluene; acetonitrile;

Reference yield:

: 142494-81-3
9,9-bis[4-(2-propenyloxy)phenyl]fluorene

: 1422984-43-7
3,3',3,3'-(5,5'-(9H-fluorene-9,9-diyl)bis(2-(oxirane-2-ylmethoxy)benzene-5,3,1-triyl))(tetrakis propane-3,1-diyl)tetrakis(triethoxysilane)

Guidance literature:: Multi-step reaction with 5 steps

1: 1,2-dichloro-benzene / 96 h / 20 - 190 °C

2: potassium carbonate / acetone / 80 °C

3: 1,2-dichloro-benzene / 8 h / 20 - 190 °C

4: potassium carbonate / acetonitrile / 20 - 80 °C

5: platinum(IV) oxide / toluene / 24 h / 85 °C / Inert atmosphere

With platinum(IV) oxide; potassium carbonate; In 1,2-dichloro-benzene; acetone; toluene; acetonitrile;