3-bromo-N-[4-chloro-2-(1-cyclopropylethylcarbamoyl)phenyl]-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

Base Information

• Chemical Name: 3-bromo-N-[4-chloro-2-(1-cyclopropylethylcarbamoyl)phenyl]-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide
• CAS No.: 1033407-59-8
• Molecular Formula: C₂₁H₁₈BrCl₂N₅O₂
• Molecular Weight: 523.216

Synonyms:3-bromo-N-[4-chloro-2-(1-cyclopropylethylcarbamoyl)phenyl]-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

Chemical Property of 3-bromo-N-[4-chloro-2-(1-cyclopropylethylcarbamoyl)phenyl]-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

Chemical Property:

Purity/Quality:

99% ,98%,Electron Grade , ^*data from raw suppliers

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Technology Process of 3-bromo-N-[4-chloro-2-(1-cyclopropylethylcarbamoyl)phenyl]-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide

There total 6 articles about 3-bromo-N-[4-chloro-2-(1-cyclopropylethylcarbamoyl)phenyl]-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-bromo-2-(3-chloro-pyridin-2-yl)-2H-pyrazole-3-carboxylic acid pentyl ester (1033407-65-6) + 2-amino-5-chloro-N-(1-cyclopropylethyl)benzamide (1033407-61-2) → 3-bromo-N-[4-chloro-2-(1-cyclopropylethylcarbamoyl)phenyl]-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide (1033407-59-8)

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 0.75h;

Reference yield:

2-amino-5-chloro-N-(1-cyclopropylethyl)benzamide (1033407-61-2) + S-benzyl 3-bromo-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carbothioate (1033407-75-8) → 3-bromo-N-[4-chloro-2-(1-cyclopropylethylcarbamoyl)phenyl]-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide (1033407-59-8)

Guidance literature:

With potassium tert-butylate; sodium sulfate; In dimethyl sulfoxide; at 20 ℃; for 1h;

Reference yield:

2-amino-5-chloro-N-(1-cyclopropylethyl)benzamide (1033407-61-2) + phenyl 3-bromo-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxylate (1033407-66-7) → 3-bromo-N-[4-chloro-2-(1-cyclopropylethylcarbamoyl)phenyl]-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carboxamide (1033407-59-8)

Guidance literature:

With potassium tert-butylate; In dimethyl sulfoxide; at 20 ℃; for 1h;

upstream raw materials:

5-bromo-2-(3-chloro-pyridin-2-yl)-2H-pyrazole-3-carboxylic acid pentyl ester

2-amino-5-chloro-N-(1-cyclopropylethyl)benzamide

3-bromo-N-(4-chloro-2-(1-cyclopropylethylcarbamoyl)phenyl)-1-(3-chloropyridin-2-yl)-4,5-dihydro-1H-pyrazole-5-carboxamide

S-benzyl 3-bromo-1-(3-chloropyridin-2-yl)-1H-pyrazole-5-carbothioate

Downstream raw materials:

3-bromo-N-[2-bromo-4-chloro-6-[[(1-cyclopropylethyl)amino]carbonyl]phenyl]-1-(3-chloro-2-pyridinyl)-1H-pyrazole-5-carboxamide

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