(2S,2''R)-1-[N-methoxycarbonyl-N-(1-methyl-2-phenylethyl)amino]-2-(methoxymethyl)pyrrolidine

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Chemical Name:(2S,2''R)-1-[N-methoxycarbonyl-N-(1-methyl-2-phenylethyl)amino]-2-(methoxymethyl)pyrrolidine
CAS No.:107300-19-6
Molecular Formula:C₁₇H₂₆N₂O₃
Molecular Weight:306.405
Hs Code.:

Synonyms:(2S,2''R)-1-[N-methoxycarbonyl-N-(1-methyl-2-phenylethyl)amino]-2-(methoxymethyl)pyrrolidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,2''R)-1-[N-methoxycarbonyl-N-(1-methyl-2-phenylethyl)amino]-2-(methoxymethyl)pyrrolidine

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Technology Process of (2S,2''R)-1-[N-methoxycarbonyl-N-(1-methyl-2-phenylethyl)amino]-2-(methoxymethyl)pyrrolidine

There total 2 articles about (2S,2''R)-1-[N-methoxycarbonyl-N-(1-methyl-2-phenylethyl)amino]-2-(methoxymethyl)pyrrolidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 72170-93-5
((S)-2-Methoxymethyl-pyrrolidin-1-yl)-[2-phenyl-eth-(E)-ylidene]-amine

: 917-54-4
methyllithium

: 79-22-1
methyl chloroformate

: 107300-19-6
(2S,2''R)-1-[N-methoxycarbonyl-N-(1-methyl-2-phenylethyl)amino]-2-(methoxymethyl)pyrrolidine

Guidance literature:: With cerium(III) chloride; Yield given. Multistep reaction; 1.) THF, 20 deg C, 2 h, 2.) THF, -78 deg C, 2 h, 3.) THF, 20 deg C, 12 h;
DOI:10.1021/ja00241a073

Reference yield:

: C₁₅H₂₄N₂O

: 79-22-1
methyl chloroformate

: 107300-19-6
(2S,2''R)-1-[N-methoxycarbonyl-N-(1-methyl-2-phenylethyl)amino]-2-(methoxymethyl)pyrrolidine

Guidance literature:: In tetrahydrofuran; diethyl ether; at 20 ℃; for 12h; optical yield given as %de; Inert atmosphere;
DOI:10.1016/j.tetasy.2010.04.042