(Z)-4-((4-oxo-3-phenyl-2-thioxothiazolidin-5-ylidene)methyl)benzoic acid

Base Information

• Chemical Name: (Z)-4-((4-oxo-3-phenyl-2-thioxothiazolidin-5-ylidene)methyl)benzoic acid
• CAS No.: 108896-17-9
• Molecular Formula: C₁₇H₁₁NO₃S₂
• Molecular Weight: 341.411

Synonyms:(Z)-4-((4-oxo-3-phenyl-2-thioxothiazolidin-5-ylidene)methyl)benzoic acid

Chemical Property of (Z)-4-((4-oxo-3-phenyl-2-thioxothiazolidin-5-ylidene)methyl)benzoic acid

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Technology Process of (Z)-4-((4-oxo-3-phenyl-2-thioxothiazolidin-5-ylidene)methyl)benzoic acid

There total 4 articles about (Z)-4-((4-oxo-3-phenyl-2-thioxothiazolidin-5-ylidene)methyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

3-phenylrhodanine (1457-46-1) + 4-Carboxybenzaldehyde (619-66-9) → (Z)-4-((4-oxo-3-phenyl-2-thioxothiazolidin-5-ylidene)methyl)benzoic acid (108896-17-9)

Guidance literature:

With ammonium acetate; acetic acid; at 180 ℃; for 0.0833333h; Microwave irradiation;

DOI:10.1021/jm400828u

Reference yield:

aniline (62-53-3) → (Z)-4-((4-oxo-3-phenyl-2-thioxothiazolidin-5-ylidene)methyl)benzoic acid (108896-17-9)

Guidance literature:

Multi-step reaction with 2 steps

1: water / 0.25 h / 160 °C / Microwave irradiation

2: ammonium acetate; acetic acid / 0.08 h / 180 °C / Microwave irradiation

With ammonium acetate; acetic acid; In water; 2: |Knoevenagel Condensation;

DOI:10.1021/jm400828u

Reference yield:

→ C17H11NO3S2 (108896-17-9)

Guidance literature:

With sodium acetate; acetic acid; at 130 ℃;

upstream raw materials:

aniline

3-phenylrhodanine

4-Carboxybenzaldehyde

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