C₃₃H₅₄O₄Si

Base Information

Chemical Name:C₃₃H₅₄O₄Si
CAS No.:1375412-37-5
Molecular Formula:C₃₃H₅₄O₄Si
Molecular Weight:542.875
Hs Code.:

C<sub>33</sub>H<sub>54</sub>O<sub>4</sub>Si

Synonyms:C₃₃H₅₄O₄Si

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Chemical Property of C₃₃H₅₄O₄Si

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Technology Process of C₃₃H₅₄O₄Si

There total 12 articles about C₃₃H₅₄O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1375412-57-9
C₃₀H₄₈O₃Si

: 123-38-6
propionaldehyde

: 1375412-37-5
C₃₃H₅₄O₄Si

Guidance literature:: With samarium diiodide; In tetrahydrofuran; at -20 ℃; for 0.833333h;
DOI:10.1002/anie.201108692

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 1375412-37-5
C₃₃H₅₄O₄Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

2.1: copper(l) iodide / tetrahydrofuran; dimethyl sulfate / 3 h / -30 °C

3.1: sodium periodate / tetrahydrofuran; water / 6 h / 20 °C

4.1: N-chloro-succinimide; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt / acetonitrile / 2.5 h / 0 °C

4.2: 0.5 h

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

5.2: 1 h / -50 - -45 °C

5.3: 2 h / -70 - 0 °C

6.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

7.1: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

With 2,6-dimethylpyridine; sodium periodate; N-chloro-succinimide; N-Bromosuccinimide; copper(l) iodide; n-butyllithium; samarium diiodide; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt; silver perchlorate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; water; acetone; dimethyl sulfate; acetonitrile; 5.3: Brook rearrangement / 7.1: Evans-Tishchenko reduction;
DOI:10.1002/anie.201108692

Reference yield:

: 1375412-52-4
C₃₃H₅₄O₂S₂Si

: 1375412-37-5
C₃₃H₅₄O₄Si

Guidance literature:: Multi-step reaction with 2 steps

1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

2: samarium diiodide / tetrahydrofuran / 0.83 h / -20 °C

With 2,6-dimethylpyridine; N-Bromosuccinimide; samarium diiodide; silver perchlorate; In tetrahydrofuran; water; acetone; 2: Evans-Tishchenko reduction;
DOI:10.1002/anie.201108692