C₃₀H₂₂Br₂S₂

Base Information

• Chemical Name: C₃₀H₂₂Br₂S₂
• CAS No.: 881636-32-4
• Molecular Formula: C₃₀H₂₂Br₂S₂
• Molecular Weight: 606.445
• Mol file: 881636-32-4.mol

Synonyms:C₃₀H₂₂Br₂S₂

Chemical Property of C₃₀H₂₂Br₂S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

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Technology Process of C₃₀H₂₂Br₂S₂

There total 1 articles about C₃₀H₂₂Br₂S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

C30H24Br2S2 → C30H22Br2S2 (881636-32-4)

Guidance literature:

With iron(III) chloride; In nitromethane; dichloromethane; for 0.0833333h;

DOI:10.1016/j.tetlet.2006.01.006

Reference yield: 65.0%

2-methyl-4-(2'-thienyl)but-3-yn-ol + C30H22Br2S2 (881636-32-4) → C42H28S4

Guidance literature:

With sodium hydroxide; copper(l) iodide; tetra-(n-butyl)ammonium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; at 80 ℃; for 24h;

DOI:10.1016/j.tetlet.2006.01.006

Reference yield:

C30H22Br2S2 (881636-32-4) → C82H68S4 (881636-37-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 65 percent / tetrabutylammonium iodide; CuI; aq. NaOH / Pd(PPh₃)4 / toluene / 24 h / 80 °C

2: 100 percent / 1,3,5-trimethyl-benzene / 24 h / Heating

With sodium hydroxide; copper(l) iodide; tetra-(n-butyl)ammonium iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In toluene; 1,3,5-trimethyl-benzene; 1: Sonogashira reaction / 2: Diels-Alder reaction and decarbonylation;

DOI:10.1016/j.tetlet.2006.01.006

Downstream raw materials:

C₈₂H₆₈S₄