C₂₉H₃₂ClF₂N₅O₄

Base Information

Chemical Name:C₂₉H₃₂ClF₂N₅O₄
CAS No.:853069-36-0
Molecular Formula:C₂₉H₃₂ClF₂N₅O₄
Molecular Weight:588.054
Hs Code.:

C<sub>29</sub>H<sub>32</sub>ClF<sub>2</sub>N<sub>5</sub>O<sub>4</sub>

Synonyms:C₂₉H₃₂ClF₂N₅O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₃₂ClF₂N₅O₄

Chemical Property:

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Technology Process of C₂₉H₃₂ClF₂N₅O₄

There total 9 articles about C₂₉H₃₂ClF₂N₅O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 853069-92-8
C₂₉H₃₃ClF₂IN₅O₄

: 853069-36-0
C₂₉H₃₂ClF₂N₅O₄

Guidance literature:: With silver (I) hydrogen carbonate; palladium diacetate; triphenylphosphine; In N,N-dimethyl-formamide; at 150 ℃; for 1h;
DOI:10.1016/j.bmc.2012.07.046

Reference yield:

: C₂₁H₂₈ClIN₄O₄

: 853069-36-0
C₂₉H₃₂ClF₂N₅O₄

Guidance literature:: Multi-step reaction with 3 steps

1.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 4 h / 0 - 20 °C

1.2: 12 h / 20 °C

2.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

3.1: silver (I) hydrogen carbonate; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 1 h / 150 °C

With oxalyl dichloride; silver (I) hydrogen carbonate; palladium diacetate; potassium carbonate; triphenylphosphine; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.07.046

Reference yield:

: 309956-78-3,172603-05-3
(R)-piperidin-3-ylcarbamic acid tert-butyl ester

: 853069-36-0
C₂₉H₃₂ClF₂N₅O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: isopropyl alcohol / 20 °C

2.1: triethylamine / 80 °C

3.1: potassium carbonate / acetonitrile / 40 °C

4.1: sodium hydride / tetrahydrofuran / 15 °C

5.1: diiodomethane; isopentyl nitrite / toluene / 80 °C

6.1: ethanol; sodium hydroxide / 80 °C

7.1: oxalyl dichloride / dichloromethane; N,N-dimethyl-formamide / 4 h / 0 - 20 °C

7.2: 12 h / 20 °C

8.1: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C

9.1: silver (I) hydrogen carbonate; palladium diacetate; triphenylphosphine / N,N-dimethyl-formamide / 1 h / 150 °C

With oxalyl dichloride; silver (I) hydrogen carbonate; diiodomethane; ethanol; palladium diacetate; sodium hydride; potassium carbonate; triethylamine; triphenylphosphine; sodium hydroxide; isopentyl nitrite; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol; toluene; acetonitrile; 5.1: |Sandmeyer Reaction;
DOI:10.1016/j.bmc.2012.07.046