2-isopropyl-4-nitrobenzoic acid 2-(2-isopropylimidazol-1-yl)ethyl ester

Base Information

Chemical Name:2-isopropyl-4-nitrobenzoic acid 2-(2-isopropylimidazol-1-yl)ethyl ester
CAS No.:1029803-93-7
Molecular Formula:C₁₈H₂₃N₃O₄
Molecular Weight:345.398
Hs Code.:

Synonyms:2-isopropyl-4-nitrobenzoic acid 2-(2-isopropylimidazol-1-yl)ethyl ester

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Chemical Property of 2-isopropyl-4-nitrobenzoic acid 2-(2-isopropylimidazol-1-yl)ethyl ester

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Technology Process of 2-isopropyl-4-nitrobenzoic acid 2-(2-isopropylimidazol-1-yl)ethyl ester

There total 5 articles about 2-isopropyl-4-nitrobenzoic acid 2-(2-isopropylimidazol-1-yl)ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 36947-68-9
2-isopropylimidazole

: 1029803-73-3
2-isopropyl-4-nitrobenzoic acid 2-bromoethyl ester

: 1029803-93-7
2-isopropyl-4-nitrobenzoic acid 2-(2-isopropylimidazol-1-yl)ethyl ester

Guidance literature:: With triethylamine; In N,N-dimethyl-formamide; for 15h; Heating / reflux;

Reference yield:

: 1029803-71-1
2-isopropyl-4-nitrobenzonitrile

: 1029803-93-7
2-isopropyl-4-nitrobenzoic acid 2-(2-isopropylimidazol-1-yl)ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; water / 1,4-dioxane / 48 h / Heating / reflux

2: sulfuric acid / 80 °C

3: triethylamine / N,N-dimethyl-formamide / 15 h / Heating / reflux

With sulfuric acid; water; triethylamine; In 1,4-dioxane; N,N-dimethyl-formamide;

Reference yield:

: 31539-91-0
N-(2-isopropyl-4-nitrophenyl)acetamide

: 1029803-93-7
2-isopropyl-4-nitrobenzoic acid 2-(2-isopropylimidazol-1-yl)ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; water / ethanol / Heating / reflux

2.1: hydrogenchloride; sodium nitrite / water / 1 h / 0 °C

2.2: 1 h / 0 - 20 °C

3.1: sulfuric acid; water / 1,4-dioxane / 48 h / Heating / reflux

4.1: sulfuric acid / 80 °C

5.1: triethylamine / N,N-dimethyl-formamide / 15 h / Heating / reflux

With hydrogenchloride; sulfuric acid; water; triethylamine; sodium nitrite; In 1,4-dioxane; ethanol; water; N,N-dimethyl-formamide;