2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone

Base Information

• Chemical Name: 2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone
• CAS No.: 85748-43-2
• Molecular Formula: C₁₇H₁₈N₄S
• Molecular Weight: 310.423
• Mol file: 85748-43-2.mol

Synonyms:2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone

Chemical Property of 2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone

There total 1 articles about 2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

phenyl(pyridin-2-yl)methanone (91-02-1) + pyrrolidine-1-carbothioic acid hydrazide (6499-14-5) → 2-benzoylpyridine N(4),N(4)-(butane-1,4-diyl)thiosemicarbazone (85748-43-2)

Guidance literature:

With sulfuric acid; In methanol; at 65 ℃; for 6h;

Reference yield: 78.0%

nickel(II) perchlorate hexahydrate + 2-benzoylpyridine N(4),N(4)-(butane-1,4-diyl)thiosemicarbazone (85748-43-2) → Ni(2-(Ph)C5H4NC N(4),(N)4-(C4H8-1,4-diyl)thiosemicarbazone)(2-(Ph)C5H4NC N(4),N(4)-(C4H8-1,4-diyl)thiosemicarbazonate)ClO4*7H2O

Guidance literature:

In methanol; chloroform; equimolar amt. of N-compd. in hot CHCl3 was added to Ni-salt soln. in hot MeOH, reflux for an hour; soln. was allowed to stand at room temp., ppt. was filtered off, washed with MeOH and ether, dried in vac. over P4O10, elem. anal.;

DOI:10.1016/j.poly.2007.09.023

Reference yield: 70.0%

2-benzoylpyridine N(4),N(4)-(butane-1,4-diyl)thiosemicarbazone (85748-43-2) + palladium dichloride → C17H18ClN4PdS

Guidance literature:

In methanol; acetone; at 60 ℃; for 72h; Sealed tube;

upstream raw materials:

phenyl(pyridin-2-yl)methanone

pyrrolidine-1-carbothioic acid hydrazide

Downstream raw materials:

[Fe(III)((2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone)^(1-))2]NO₃