2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone

Base Information

Chemical Name:2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone
CAS No.:85748-43-2
Molecular Formula:C₁₇H₁₈N₄S
Molecular Weight:310.423
Hs Code.:

2-benzoylpyridine N<sup>(4)</sup>,N<sup>(4)</sup>-(butane-1,4-diyl)thiosemicarbazone

Synonyms:2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone

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Technology Process of 2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone

There total 1 articles about 2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 91-02-1
phenyl(pyridin-2-yl)methanone

: 6499-14-5
pyrrolidine-1-carbothioic acid hydrazide

: 85748-43-2
2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone

Guidance literature:: With sulfuric acid; In methanol; at 65 ℃; for 6h;

Reference yield: 78.0%

: nickel(II) perchlorate hexahydrate

: 85748-43-2
2-benzoylpyridine N⁽⁴⁾,N⁽⁴⁾-(butane-1,4-diyl)thiosemicarbazone

: Ni(2-(Ph)C₅H₄NC N⁽⁴⁾,(N)4-(C₄H₈-1,4-diyl)thiosemicarbazone)(2-(Ph)C₅H₄NC N⁽⁴⁾,N⁽⁴⁾-(C₄H₈-1,4-diyl)thiosemicarbazonate)ClO₄*7H₂O

Guidance literature:: In methanol; chloroform; equimolar amt. of N-compd. in hot CHCl3 was added to Ni-salt soln. in hot MeOH, reflux for an hour; soln. was allowed to stand at room temp., ppt. was filtered off, washed with MeOH and ether, dried in vac. over P4O10, elem. anal.;
DOI:10.1016/j.poly.2007.09.023