6,8,9,11,12,14,15,17,18,20,21,23,24,26-tetradecahydro-6-methyl-6-<2-(phenylmethoxy)ethyl>-<1,4>benzodioxino<2,3-c><1,6,9,12,15,18,21>-heptaoxacyclotricosin

Base Information

Chemical Name:6,8,9,11,12,14,15,17,18,20,21,23,24,26-tetradecahydro-6-methyl-6-<2-(phenylmethoxy)ethyl>-<1,4>benzodioxino<2,3-c><1,6,9,12,15,18,21>-heptaoxacyclotricosin
CAS No.:123295-34-1
Molecular Formula:C₃₂H₄₄O₁₀
Molecular Weight:588.695
Hs Code.:

6,8,9,11,12,14,15,17,18,20,21,23,24,26-tetradecahydro-6-methyl-6-<2-(phenylmethoxy)ethyl>-<1,4>benzodioxino<2,3-c><1,6,9,12,15,18,21>-heptaoxacyclotricosin

Synonyms:6,8,9,11,12,14,15,17,18,20,21,23,24,26-tetradecahydro-6-methyl-6-<2-(phenylmethoxy)ethyl>-<1,4>benzodioxino<2,3-c><1,6,9,12,15,18,21>-heptaoxacyclotricosin

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Chemical Property of 6,8,9,11,12,14,15,17,18,20,21,23,24,26-tetradecahydro-6-methyl-6-<2-(phenylmethoxy)ethyl>-<1,4>benzodioxino<2,3-c><1,6,9,12,15,18,21>-heptaoxacyclotricosin

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Technology Process of 6,8,9,11,12,14,15,17,18,20,21,23,24,26-tetradecahydro-6-methyl-6-<2-(phenylmethoxy)ethyl>-<1,4>benzodioxino<2,3-c><1,6,9,12,15,18,21>-heptaoxacyclotricosin

There total 3 articles about 6,8,9,11,12,14,15,17,18,20,21,23,24,26-tetradecahydro-6-methyl-6-<2-(phenylmethoxy)ethyl>-<1,4>benzodioxino<2,3-c><1,6,9,12,15,18,21>-heptaoxacyclotricosin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 81279-78-9
α-methyl-2-<2-(phenylmethoxy)ethyl>-1,4-benzodioxin-2,3-dimethanol

: 19249-03-7
triethylene glycol di-(p-toluenesulfonate)

: 123295-34-1
6,8,9,11,12,14,15,17,18,20,21,23,24,26-tetradecahydro-6-methyl-6-<2-(phenylmethoxy)ethyl>-<1,4>benzodioxino<2,3-c><1,6,9,12,15,18,21>-heptaoxacyclotricosin

Guidance literature:: With sodium hydride; Multistep reaction; 1.) THF, reflux, 2 h, 2.) THF, reflux, 24 h;

Reference yield:

: 67471-01-6
1,4-benzodioxin-2-carboxylic acid

: 123295-34-1
6,8,9,11,12,14,15,17,18,20,21,23,24,26-tetradecahydro-6-methyl-6-<2-(phenylmethoxy)ethyl>-<1,4>benzodioxino<2,3-c><1,6,9,12,15,18,21>-heptaoxacyclotricosin

Guidance literature:: Multi-step reaction with 3 steps

2: 90 percent / LiAlH₄ / diethyl ether / Ambient temperature

3: 1.) NaH / 1.) THF, reflux, 2 h, 2.) THF, reflux, 24 h

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether;

Reference yield:

: 123295-18-1
3-methyl-3-<2-(phenylmethoxy)ethyl>-furo<3,4-b><1,4>benzodioxin-1 (3H)-one

: 123295-34-1
6,8,9,11,12,14,15,17,18,20,21,23,24,26-tetradecahydro-6-methyl-6-<2-(phenylmethoxy)ethyl>-<1,4>benzodioxino<2,3-c><1,6,9,12,15,18,21>-heptaoxacyclotricosin

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / LiAlH₄ / diethyl ether / Ambient temperature

2: 1.) NaH / 1.) THF, reflux, 2 h, 2.) THF, reflux, 24 h

With lithium aluminium tetrahydride; sodium hydride; In diethyl ether;