N¹-benzyl-N³-[4-(3-(4-chlorophenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl)benzenesulfonyl]thiourea

Base Information

• Chemical Name: N¹-benzyl-N³-[4-(3-(4-chlorophenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl)benzenesulfonyl]thiourea
• CAS No.: 911682-09-2
• Molecular Formula: C₃₀H₂₅ClN₄O₂S₂
• Molecular Weight: 573.139

Synonyms:N¹-benzyl-N³-[4-(3-(4-chlorophenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl)benzenesulfonyl]thiourea

Chemical Property of N¹-benzyl-N³-[4-(3-(4-chlorophenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl)benzenesulfonyl]thiourea

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Technology Process of N¹-benzyl-N³-[4-(3-(4-chlorophenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl)benzenesulfonyl]thiourea

There total 4 articles about N¹-benzyl-N³-[4-(3-(4-chlorophenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl)benzenesulfonyl]thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

Benzyl isothiocyanate (622-78-6) + 4-[3-(4-chloro-phenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl]-benzenesulfonamide (263903-63-5) → N1-benzyl-N3-[4-(3-(4-chlorophenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl)benzenesulfonyl]thiourea (911682-09-2)

Guidance literature:

With potassium carbonate; In acetone; for 10h; Heating;

DOI:10.1016/j.bmc.2006.06.020

Reference yield:

(E)-2-(4-chlorobenzylidene)-indan-1-one (5706-17-2) → N1-benzyl-N3-[4-(3-(4-chlorophenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl)benzenesulfonyl]thiourea (911682-09-2)

Guidance literature:

Multi-step reaction with 2 steps

1: 85 percent / ethanol / 4 h / Heating

2: 78 percent / potassium carbonate / acetone / 10 h / Heating

With potassium carbonate; In ethanol; acetone;

DOI:10.1016/j.bmc.2006.06.020

Reference yield:

4-chlorobenzaldehyde (104-88-1) → N1-benzyl-N3-[4-(3-(4-chlorophenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl)benzenesulfonyl]thiourea (911682-09-2)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium hydroxide / ethanol; H₂O

2: 85 percent / ethanol / 4 h / Heating

3: 78 percent / potassium carbonate / acetone / 10 h / Heating

With sodium hydroxide; potassium carbonate; In ethanol; water; acetone;

DOI:10.1016/j.bmc.2006.06.020

upstream raw materials:

Benzyl isothiocyanate

4-[3-(4-chloro-phenyl)-3a,4-dihydro-3H-indeno[1,2-c]pyrazol-2-yl]-benzenesulfonamide

(E)-2-(4-chlorobenzylidene)-indan-1-one

4-chlorobenzaldehyde

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