ethyl (1R,2S,6R)-1-(4-methylpent-3-enyl)-2-hydroxy-6-methylcyclohexanecarboxylate

Base Information

Chemical Name:ethyl (1R,2S,6R)-1-(4-methylpent-3-enyl)-2-hydroxy-6-methylcyclohexanecarboxylate
CAS No.:127982-50-7
Molecular Formula:C₁₆H₂₈O₃
Molecular Weight:268.397
Hs Code.:

Synonyms:ethyl (1R,2S,6R)-1-(4-methylpent-3-enyl)-2-hydroxy-6-methylcyclohexanecarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl (1R,2S,6R)-1-(4-methylpent-3-enyl)-2-hydroxy-6-methylcyclohexanecarboxylate

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Technology Process of ethyl (1R,2S,6R)-1-(4-methylpent-3-enyl)-2-hydroxy-6-methylcyclohexanecarboxylate

There total 2 articles about ethyl (1R,2S,6R)-1-(4-methylpent-3-enyl)-2-hydroxy-6-methylcyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 43161-11-1
5-iodo-2-methylpent-2-ene

: 127982-49-4
(+)-ethyl (1R,2S,6R)-2-hydroxy-6-methylcyclohexanecarboxylate

: 127982-50-7
ethyl (1R,2S,6R)-1-(4-methylpent-3-enyl)-2-hydroxy-6-methylcyclohexanecarboxylate

Guidance literature:: With lithium diisopropyl amide; 1.) THF, -50 deg C, 10 min, 2.) THF/HMPTA, reflux, 10 min;
DOI:10.1002/hlca.19890720821

Reference yield:

: rac-ethyl 2-methyl-6-oxocyclohexanecarboxylate

: 127982-50-7
ethyl (1R,2S,6R)-1-(4-methylpent-3-enyl)-2-hydroxy-6-methylcyclohexanecarboxylate

Guidance literature:: Multi-step reaction with 2 steps

2: 80 percent / LDA / 1.) THF, -50 deg C, 10 min, 2.) THF/HMPTA, reflux, 10 min

With lithium diisopropyl amide;
DOI:10.1002/hlca.19890720821