pentafluorobenzyl (N,N-isopropyl-p-chlorophenyl)carbamate

Base Information

• Chemical Name: pentafluorobenzyl (N,N-isopropyl-p-chlorophenyl)carbamate
• CAS No.: 125489-17-0
• Molecular Formula: C₁₇H₁₃ClF₅NO₂
• Molecular Weight: 393.741
• Mol file: 125489-17-0.mol

Synonyms:pentafluorobenzyl (N,N-isopropyl-p-chlorophenyl)carbamate

Chemical Property of pentafluorobenzyl (N,N-isopropyl-p-chlorophenyl)carbamate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of pentafluorobenzyl (N,N-isopropyl-p-chlorophenyl)carbamate

There total 3 articles about pentafluorobenzyl (N,N-isopropyl-p-chlorophenyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

N-(4-chlorophenyl)-N-isopropylamine (770-40-1) + 2,3,4,5,6-pentafluorobenzyl chloroformate (53526-74-2) → pentafluorobenzyl (N,N-isopropyl-p-chlorophenyl)carbamate (125489-17-0)

Guidance literature:

With sodium carbonate; In water; acetone; at 20 ℃; for 5h;

DOI:10.1007/BF00978460

Reference yield:

(2,3,4,5,6-pentafluorophenyl)methanol (440-60-8) → pentafluorobenzyl (N,N-isopropyl-p-chlorophenyl)carbamate (125489-17-0)

Guidance literature:

Multi-step reaction with 2 steps

1: diethyl ether / 2 h / 0 °C

2: 78 percent / Na₂CO₃ / H₂O; acetone / 5 h / 20 °C

With sodium carbonate; In diethyl ether; water; acetone;

DOI:10.1007/BF00978460

Reference yield:

4-chloro-aniline (106-47-8) → pentafluorobenzyl (N,N-isopropyl-p-chlorophenyl)carbamate (125489-17-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 2 h / Heating

2: 78 percent / Na₂CO₃ / H₂O; acetone / 5 h / 20 °C

With sodium carbonate; In water; acetone;

DOI:10.1007/BF00978460

upstream raw materials:

N-(4-chlorophenyl)-N-isopropylamine

2,3,4,5,6-pentafluorobenzyl chloroformate

(2,3,4,5,6-pentafluorophenyl)methanol

4-chloro-aniline