(S)-3-aminomethyl-5-methyl-hexanoic acid 1-cyclohexyloxycarbonyloxy-ethyl ester trifluoroacetate

Base Information

Chemical Name:(S)-3-aminomethyl-5-methyl-hexanoic acid 1-cyclohexyloxycarbonyloxy-ethyl ester trifluoroacetate
CAS No.:1026789-25-2
Molecular Formula:C₂HF₃O₂*C₁₇H₃₁NO₅
Molecular Weight:443.461
Hs Code.:

Synonyms:(S)-3-aminomethyl-5-methyl-hexanoic acid 1-cyclohexyloxycarbonyloxy-ethyl ester trifluoroacetate

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Chemical Property of (S)-3-aminomethyl-5-methyl-hexanoic acid 1-cyclohexyloxycarbonyloxy-ethyl ester trifluoroacetate

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Technology Process of (S)-3-aminomethyl-5-methyl-hexanoic acid 1-cyclohexyloxycarbonyloxy-ethyl ester trifluoroacetate

There total 4 articles about (S)-3-aminomethyl-5-methyl-hexanoic acid 1-cyclohexyloxycarbonyloxy-ethyl ester trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1026789-36-5
(S)-3-(tert-butoxycarbonylamino-methyl)-5-rnethyl-hexanoic acid 1-cyclohexyloxycarbonyloxy-ethyl ester

: 76-05-1
trifluoroacetic acid

: 1026789-25-2
(S)-3-aminomethyl-5-methyl-hexanoic acid 1-cyclohexyloxycarbonyloxy-ethyl ester trifluoroacetate

Guidance literature:: In dichloromethane; at 0 - 20 ℃; for 5h;

Reference yield:

: 95789-69-8,102672-57-1
cyclohexyl (1-iodoethyl)carbonate

: 1026789-25-2
(S)-3-aminomethyl-5-methyl-hexanoic acid 1-cyclohexyloxycarbonyloxy-ethyl ester trifluoroacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: caesium carbonate / methanol / 4 h / 20 °C

1.2: 20 °C

2.1: dichloromethane / 20 °C / Cooling with ice

With caesium carbonate; In methanol; dichloromethane;

Reference yield:

: 99464-83-2
1-chloroethyl cyclohexyl carbonate

: 1026789-25-2
(S)-3-aminomethyl-5-methyl-hexanoic acid 1-cyclohexyloxycarbonyloxy-ethyl ester trifluoroacetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium iodide / acetonitrile / 5.5 h / 50 °C

2.1: caesium carbonate / methanol / 4 h / 20 °C

2.2: 20 °C

3.1: dichloromethane / 20 °C / Cooling with ice

With caesium carbonate; sodium iodide; In methanol; dichloromethane; acetonitrile;