(2S,3RS)-N-phthaloyl-3-bromo-3-(4-fluoro-3-nitrophenyl)alanine methyl ester

Base Information

Chemical Name:(2S,3RS)-N-phthaloyl-3-bromo-3-(4-fluoro-3-nitrophenyl)alanine methyl ester
CAS No.:230313-39-0
Molecular Formula:C₁₈H₁₂BrFN₂O₆
Molecular Weight:451.205
Hs Code.:

Synonyms:(2S,3RS)-N-phthaloyl-3-bromo-3-(4-fluoro-3-nitrophenyl)alanine methyl ester

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Chemical Property of (2S,3RS)-N-phthaloyl-3-bromo-3-(4-fluoro-3-nitrophenyl)alanine methyl ester

Chemical Property:

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Technology Process of (2S,3RS)-N-phthaloyl-3-bromo-3-(4-fluoro-3-nitrophenyl)alanine methyl ester

There total 4 articles about (2S,3RS)-N-phthaloyl-3-bromo-3-(4-fluoro-3-nitrophenyl)alanine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 230313-38-9
(S)-N-phthaloyl-3-(4-fluoro-3-nitrophenyl)alanine methyl ester

: 230313-39-0
(2S,3RS)-N-phthaloyl-3-bromo-3-(4-fluoro-3-nitrophenyl)alanine methyl ester

Guidance literature:: With N-Bromosuccinimide; In tetrachloromethane; for 6h; Heating; irradiation;
DOI:10.1021/ol9906054

Reference yield:

: (S)-4-fluoro-3-nitrophenylalanine

: 230313-39-0
(2S,3RS)-N-phthaloyl-3-bromo-3-(4-fluoro-3-nitrophenyl)alanine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: Na₂CO₃ / H₂O / 1 h

2: 238 mg / thionyl chloride / 16 h

3: 100 percent / NBS / CCl₄ / 6 h / Heating; irradiation

With N-Bromosuccinimide; thionyl chloride; sodium carbonate; In tetrachloromethane; water;
DOI:10.1021/ol9906054

Reference yield:

: C₁₇H₁₁FN₂O₆

: 230313-39-0
(2S,3RS)-N-phthaloyl-3-bromo-3-(4-fluoro-3-nitrophenyl)alanine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 238 mg / thionyl chloride / 16 h

2: 100 percent / NBS / CCl₄ / 6 h / Heating; irradiation

With N-Bromosuccinimide; thionyl chloride; In tetrachloromethane;
DOI:10.1021/ol9906054