4-Toluoliminosulfonsaeure-dimethylamid

Base Information

• Chemical Name: 4-Toluoliminosulfonsaeure-dimethylamid
• CAS No.: 92939-24-7
• Molecular Formula: C₉H₁₄N₂OS
• Molecular Weight: 198.289
• Mol file: 92939-24-7.mol

Synonyms:4-Toluoliminosulfonsaeure-dimethylamid

Chemical Property of 4-Toluoliminosulfonsaeure-dimethylamid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-Toluoliminosulfonsaeure-dimethylamid

There total 10 articles about 4-Toluoliminosulfonsaeure-dimethylamid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C16H18N2O2S (1050610-05-3) → 4-Toluoliminosulfonsaeure-dimethylamid (92939-24-7)

Guidance literature:

In ethanol; for 2h; heating on a water bath;

Reference yield:

4-methylbenzenesulfinyl chloride (10439-23-3) → 4-Toluoliminosulfonsaeure-dimethylamid (92939-24-7)

Guidance literature:

Multi-step reaction with 3 steps

1: (i) Py, (ii) tBuOCl

3: H₂SO₄

With sulfuric acid;

DOI:10.1021/ja00814a031

Reference yield:

C9H14N2OS (52720-06-6) → 4-Toluoliminosulfonsaeure-dimethylamid (92939-24-7)

Guidance literature:

Multi-step reaction with 2 steps

1: Py

2: H₂SO₄

With pyridine; sulfuric acid;

DOI:10.1021/ja00814a031

upstream raw materials:

C₁₆H₁₈N₂O₂S

N-benzoyl-p-toluene sulfonimidoyl chloride

4-methylbenzenesulfinyl chloride

C₉H₁₄N₂OS

Downstream raw materials:

C₉H₁₃ClN₂OS

Refernces

• 1、 Levchenko, E. S.,Slyusarenko, E. I.,Kalinin, V. N.. "DERIVATIVES OF SULFONIMIDIC ACIDS. N1,N1-DIALKYL-N2-CHLOROARENESULFONIMIDAMIDES". . p. 1802 - 1805. Retrieved 2007/10/02.