2-benzylcyclohexanone oxime acetate

Base Information

Chemical Name:2-benzylcyclohexanone oxime acetate
CAS No.:119220-51-8
Molecular Formula:C₁₅H₁₉NO₂
Molecular Weight:245.321
Hs Code.:

Synonyms:2-benzylcyclohexanone oxime acetate

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Chemical Property of 2-benzylcyclohexanone oxime acetate

Chemical Property:

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Technology Process of 2-benzylcyclohexanone oxime acetate

There total 6 articles about 2-benzylcyclohexanone oxime acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 119220-47-2,119220-48-3
C₁₈H₂₇NO₂Si

: 119220-51-8
2-benzylcyclohexanone oxime acetate

: 119220-50-7
(E)-7-phenylhept-6-enenitrile

Guidance literature:: With cesium fluoride; In acetonitrile; at 70 ℃; for 8h;
DOI:10.1016/S0040-4020(01)81693-8

Reference yield:

: 770-09-2
benzyltrimethylsilane

: 119220-51-8
2-benzylcyclohexanone oxime acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-butyllithium, N,N,N',N'-tetramethylethylenediamine / 1.) THF, hexane, -78 deg C, 0 deg C, 30 min, 2.) THF, hexane, -78 deg C, -15 deg C, 4 h

2: 795 mg / CrO₃ / pyridine; CH₂Cl₂ / 4 h

3: 96 percent / HONH₂*HCl, NaOAc / ethanol / 3 h / Ambient temperature

4: 97 percent / pyridine; CH₂Cl₂ / 2 h / 0 °C

5: 8.8 mg / CsF / acetonitrile / 8 h / 70 °C

With chromium(VI) oxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydroxylamine hydrochloride; sodium acetate; cesium fluoride; In pyridine; ethanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)81693-8

Reference yield:

: 286-20-4
cyclohexane-1,2-epoxide

: 119220-51-8
2-benzylcyclohexanone oxime acetate

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) n-butyllithium, N,N,N',N'-tetramethylethylenediamine / 1.) THF, hexane, -78 deg C, 0 deg C, 30 min, 2.) THF, hexane, -78 deg C, -15 deg C, 4 h

2: 795 mg / CrO₃ / pyridine; CH₂Cl₂ / 4 h

3: 96 percent / HONH₂*HCl, NaOAc / ethanol / 3 h / Ambient temperature

4: 97 percent / pyridine; CH₂Cl₂ / 2 h / 0 °C

5: 8.8 mg / CsF / acetonitrile / 8 h / 70 °C

With chromium(VI) oxide; n-butyllithium; N,N,N,N,-tetramethylethylenediamine; hydroxylamine hydrochloride; sodium acetate; cesium fluoride; In pyridine; ethanol; dichloromethane; acetonitrile;
DOI:10.1016/S0040-4020(01)81693-8