N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(1H-imidazol-4-yl)acetamide)

Base Information

Chemical Name:N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(1H-imidazol-4-yl)acetamide)
CAS No.:1610728-66-9
Molecular Formula:C₂₀H₂₂N₁₀O₂S₂
Molecular Weight:498.592
Hs Code.:

Synonyms:N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(1H-imidazol-4-yl)acetamide)

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Chemical Property of N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(1H-imidazol-4-yl)acetamide)

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Technology Process of N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(1H-imidazol-4-yl)acetamide)

There total 5 articles about N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(1H-imidazol-4-yl)acetamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1610728-92-1
5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazol-2-amine)

: 51718-80-0
methyl 2-(1H-imidazol-4-yl)acetate hydrochloride

: 1610728-66-9
N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(1H-imidazol-4-yl)acetamide)

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 130 ℃; for 0.75h; Microwave irradiation;

Reference yield:

: 1610728-91-0
(S,S)-dibenzyl cyclohexyl 1,3-dicarboxylate

: 1610728-66-9
N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(1H-imidazol-4-yl)acetamide)

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 0.33 h

2: trichlorophosphate / 3 h / 40 - 80 °C

3: caesium carbonate / N,N-dimethyl-formamide / 0.75 h / 130 °C / Microwave irradiation

With palladium 10% on activated carbon; hydrogen; caesium carbonate; trichlorophosphate; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 2305-30-8,2305-31-9,3971-31-1,21917-23-7,116724-13-1,116724-14-2
trans-e,a-1,3-cyclohexanedicarboxylic acid

: 1610728-66-9
N,N'-(5,5'-((1S,3S)-cyclohexane-1,3-diyl)bis(1,3,4-thiadiazole-5,2-diyl))bis(2-(1H-imidazol-4-yl)acetamide)

Guidance literature:: Multi-step reaction with 2 steps

1: trichlorophosphate / 3 h / 40 - 80 °C

2: caesium carbonate / N,N-dimethyl-formamide / 0.75 h / 130 °C / Microwave irradiation

With caesium carbonate; trichlorophosphate; In N,N-dimethyl-formamide;