(2R,3S,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-iodo-3,4-dihydro-2H-pyran

Base Information

Chemical Name:(2R,3S,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-iodo-3,4-dihydro-2H-pyran
CAS No.:1365092-15-4
Molecular Formula:C₂₇H₂₇IO₄
Molecular Weight:542.413
Hs Code.:

Synonyms:(2R,3S,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-iodo-3,4-dihydro-2H-pyran

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Chemical Property of (2R,3S,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-iodo-3,4-dihydro-2H-pyran

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Technology Process of (2R,3S,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-iodo-3,4-dihydro-2H-pyran

There total 3 articles about (2R,3S,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-iodo-3,4-dihydro-2H-pyran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 80040-79-5
3,4,6-tri-O-benzyl-D-galactal

: 1365092-15-4
(2R,3S,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-iodo-3,4-dihydro-2H-pyran

Guidance literature:: With N-iodo-succinimide; silver nitrate; In acetonitrile; at 80 ℃; for 0.5h; Inert atmosphere;
DOI:10.1021/ol500039s

Reference yield: 63.0%

: 55628-54-1,80040-79-5,71049-35-9
(2R,3S,4S)-3,4-bis(benzyloxy)-2-(benzyloxymethyl)-3,4-dihydro-2H-pyran

: 1365092-15-4
(2R,3S,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-iodo-3,4-dihydro-2H-pyran

Guidance literature:: With N-iodo-succinimide; silver nitrate; In acetonitrile; at 80 ℃; for 1.5h; Inert atmosphere;
DOI:10.1002/ejoc.202000494

Reference yield:

: C₂₇H₂₉IO₅

: 1365092-15-4
(2R,3S,4S)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)-5-iodo-3,4-dihydro-2H-pyran

Guidance literature:: C₂₇H₂₉IO₅; With 1,1'-sulfinylbisbenzene; 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -78 ℃; for 0.5h; Inert atmosphere; Molecular sieve;

With trifluoromethylsulfonic anhydride; In dichloromethane; at -78 - 20 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/ol3003139