C₃₈H₄₆O₅Si

Base Information

Chemical Name:C₃₈H₄₆O₅Si
CAS No.:1592771-23-7
Molecular Formula:C₃₈H₄₆O₅Si
Molecular Weight:610.866
Hs Code.:

C<sub>38</sub>H<sub>46</sub>O<sub>5</sub>Si

Synonyms:C₃₈H₄₆O₅Si

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Chemical Property of C₃₈H₄₆O₅Si

Chemical Property:

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Technology Process of C₃₈H₄₆O₅Si

There total 6 articles about C₃₈H₄₆O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: methyl 3,5-O-di(tert-butyl)silylene-2-deoxy-D-ribofuranoside

: 1592771-23-7
C₃₈H₄₆O₅Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 1 h / 0 °C / Inert atmosphere

2.1: 4-methyl-morpholine / dichloromethane / 1 h / 20 °C / Inert atmosphere

3.1: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 21 h / 20 °C

4.1: samarium diiodide / tetrahydrofuran; methanol / 0.5 h / -20 °C / Inert atmosphere

5.1: lithium borohydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

6.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.33 h / 0 °C / Inert atmosphere

6.2: 1 h / 0 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

8.1: 1H-imidazole / N,N-dimethyl-formamide / 1.5 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; 1H-imidazole; lithium borohydride; samarium diiodide; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; sodium hydrogencarbonate; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 2.1: |Michael Addition;
DOI:10.1021/ol500788c

Reference yield:

: C₁₈H₃₂O₆Si

: 1592771-23-7
C₃₈H₄₆O₅Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: samarium diiodide / tetrahydrofuran; methanol / 0.5 h / -20 °C / Inert atmosphere

2.1: lithium borohydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

3.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.33 h / 0 °C / Inert atmosphere

3.2: 1 h / 0 °C / Inert atmosphere

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

5.1: 1H-imidazole / N,N-dimethyl-formamide / 1.5 h / 0 °C / Inert atmosphere

With 1H-imidazole; lithium borohydride; samarium diiodide; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; toluene;
DOI:10.1021/ol500788c

Reference yield:

: 1592771-15-7
C₁₆H₃₂O₃S₂Si

: 1592771-23-7
C₃₈H₄₆O₅Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 4-methyl-morpholine / dichloromethane / 1 h / 20 °C / Inert atmosphere

2.1: methyl iodide; sodium hydrogencarbonate / acetonitrile; water / 21 h / 20 °C

3.1: samarium diiodide / tetrahydrofuran; methanol / 0.5 h / -20 °C / Inert atmosphere

4.1: lithium borohydride / tetrahydrofuran / 1 h / 20 °C / Inert atmosphere

5.1: potassium hexamethylsilazane / tetrahydrofuran; toluene / 0.33 h / 0 °C / Inert atmosphere

5.2: 1 h / 0 °C / Inert atmosphere

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C

7.1: 1H-imidazole / N,N-dimethyl-formamide / 1.5 h / 0 °C / Inert atmosphere

With 4-methyl-morpholine; 1H-imidazole; lithium borohydride; samarium diiodide; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; sodium hydrogencarbonate; methyl iodide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; toluene; acetonitrile; 1.1: |Michael Addition;
DOI:10.1021/ol500788c