1-(o-hydroxyphenyl)-3-cyclohexylpropargylic alcohol

Base Information

Chemical Name:1-(o-hydroxyphenyl)-3-cyclohexylpropargylic alcohol
CAS No.:1322775-85-8
Molecular Formula:C₁₅H₁₈O₂
Molecular Weight:230.307
Hs Code.:

Synonyms:1-(o-hydroxyphenyl)-3-cyclohexylpropargylic alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(o-hydroxyphenyl)-3-cyclohexylpropargylic alcohol

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Technology Process of 1-(o-hydroxyphenyl)-3-cyclohexylpropargylic alcohol

There total 1 articles about 1-(o-hydroxyphenyl)-3-cyclohexylpropargylic alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 931-48-6
2-cyclohexylacetylene

: 90-02-8
salicylaldehyde

: 1322775-85-8
1-(o-hydroxyphenyl)-3-cyclohexylpropargylic alcohol

Guidance literature:: 2-cyclohexylacetylene; With n-butyllithium; In tetrahydrofuran; at -78 - -40 ℃; for 4h;

salicylaldehyde; In tetrahydrofuran; at -78 ℃; for 12h;
DOI:10.1021/ol503662g

Reference yield: 85.0%

: 1322775-85-8
1-(o-hydroxyphenyl)-3-cyclohexylpropargylic alcohol

: 2-(cyclohexylmethyl)benzofuran

Guidance literature:: With tert-butylisonitrile; palladium diacetate; caesium carbonate; In acetonitrile; at 20 ℃; for 15h;
DOI:10.1021/acs.joc.5b02204

Reference yield: 77.0%

: 1322775-85-8
1-(o-hydroxyphenyl)-3-cyclohexylpropargylic alcohol

: 213272-97-0
N-(3,4-dihydro-1-naphthyl)acetamide

: N-((6aS,7R,12aR)-7-(cyclohexylethynyl)-5,6,6a,7-tetrahydro-12aH-benzo[c]xanthen-12a-yl)acetamide

Guidance literature:: With ((R)-3,3'-bis(pentamethylphenyl)-1,1'-binaphthyl-2,2'-diyl) hydrogenphosphate; In dichloromethane; at 20 ℃; for 16h; enantioselective reaction;
DOI:10.1021/ol503662g