N'--N-p-tolyl-diimid-N-oxid

Base Information

• Chemical Name: N'--N-p-tolyl-diimid-N-oxid
• CAS No.: 15925-33-4
• Molecular Formula: C₁₄H₁₄N₂O₄S
• Molecular Weight: 306.342

Synonyms:N'--N-p-tolyl-diimid-N-oxid

Chemical Property of N'--N-p-tolyl-diimid-N-oxid

Chemical Property:

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Technology Process of N'--N-p-tolyl-diimid-N-oxid

There total 1 articles about N'--N-p-tolyl-diimid-N-oxid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4-methylphenyl)hydroxylamine (623-10-9) + p-toluenesulfonyl chloride (98-59-9) → N'--N-p-tolyl-diimid-N-oxid (15925-33-4)

Guidance literature:

Multistep reaction; (i) NH₃, nBuNO₂, Et₂O, (ii) /BRN= 607898/, aq. NaHCO₃;

DOI:10.1021/jo01025a014

Reference yield:

N'--N-p-tolyl-diimid-N-oxid (15925-33-4) → N'-<4-Chlor-phenyl>-N-p-tolyl-diimid-N-oxid (96295-23-7)

Guidance literature:

In dichloromethane;

DOI:10.1021/jo01025a014

upstream raw materials:

N-(4-methylphenyl)hydroxylamine

p-toluenesulfonyl chloride

Downstream raw materials:

N'-<4-Chlor-phenyl>-N-p-tolyl-diimid-N-oxid

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