4-(2-tert-butoxycarbonylaminoethylamino)-3-naphthalen-2-ylbenzoic acid methyl ester

Base Information

Chemical Name:4-(2-tert-butoxycarbonylaminoethylamino)-3-naphthalen-2-ylbenzoic acid methyl ester
CAS No.:1032373-59-3
Molecular Formula:C₂₅H₂₈N₂O₄
Molecular Weight:420.508
Hs Code.:

Synonyms:4-(2-tert-butoxycarbonylaminoethylamino)-3-naphthalen-2-ylbenzoic acid methyl ester

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Chemical Property of 4-(2-tert-butoxycarbonylaminoethylamino)-3-naphthalen-2-ylbenzoic acid methyl ester

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Technology Process of 4-(2-tert-butoxycarbonylaminoethylamino)-3-naphthalen-2-ylbenzoic acid methyl ester

There total 1 articles about 4-(2-tert-butoxycarbonylaminoethylamino)-3-naphthalen-2-ylbenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 1032373-57-1
4-amino-3-naphthalen-2-ylbenzoic acid methyl ester

: 89711-08-0
N-(t-butoxycarbonyl)glycinal

: 1032373-59-3
4-(2-tert-butoxycarbonylaminoethylamino)-3-naphthalen-2-ylbenzoic acid methyl ester

Guidance literature:: 4-amino-3-naphthalen-2-ylbenzoic acid methyl ester; N-(t-butoxycarbonyl)glycinal; With acetic acid; In methanol; at 20 ℃; for 1h; Molecular sieve; Inert atmosphere;

With sodium cyanoborohydride; In methanol; at 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.bmc.2008.09.058

Reference yield:

: 1032373-59-3
4-(2-tert-butoxycarbonylaminoethylamino)-3-naphthalen-2-ylbenzoic acid methyl ester

: 1032373-63-9
4-(2-tert-butoxycarbonylaminoethylamino)-3-naphthalen-2-ylbenzoic acid

Guidance literature:: 4-(2-tert-butoxycarbonylaminoethylamino)-3-naphthalen-2-ylbenzoic acid methyl ester; With lithium hydroxide; water; In tetrahydrofuran; Reflux;

With hydrogenchloride; water; In ethyl acetate;
DOI:10.1016/j.bmc.2008.09.058