[5-butyl-15-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II)

Base Information

• Chemical Name: [5-butyl-15-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II)
• CAS No.: 1268697-65-9
• Molecular Formula: C₄₄H₄₃BN₄O₂Zn
• Molecular Weight: 736.052

Synonyms:[5-butyl-15-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II)

Chemical Property of [5-butyl-15-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II)

Chemical Property:

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Technology Process of [5-butyl-15-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II)

There total 5 articles about [5-butyl-15-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

[5-bromo-15-(n-butyl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II) (1268697-60-4) + 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane (25015-63-8) → [5-butyl-15-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II) (1268697-65-9)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; In 1,2-dichloro-ethane; for 12h;

DOI:10.1016/j.tet.2010.12.025

Reference yield:

C38H34N4 → [5-butyl-15-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II) (1268697-65-9)

Guidance literature:

Multi-step reaction with 3 steps

1: N-Bromosuccinimide

2: zinc diacetate

3: bis-triphenylphosphine-palladium(II) chloride / 1,2-dichloro-ethane / 12 h

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; zinc diacetate; In 1,2-dichloro-ethane;

DOI:10.1016/j.tet.2010.12.025

Reference yield:

5-bromo-15-butyl-10,20-di-p-tolylporphyrin (1063613-06-8) → [5-butyl-15-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II) (1268697-65-9)

Guidance literature:

Multi-step reaction with 2 steps

1: zinc diacetate

2: bis-triphenylphosphine-palladium(II) chloride / 1,2-dichloro-ethane / 12 h

With bis-triphenylphosphine-palladium(II) chloride; zinc diacetate; In 1,2-dichloro-ethane;

DOI:10.1016/j.tet.2010.12.025

upstream raw materials:

5-bromo-15-butyl-10,20-di-p-tolylporphyrin

[5-bromo-15-(n-butyl)-10,20-bis(4-methylphenyl)porphyrinato]zinc(II)

4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

5-butyl-15-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)-10,20-bis(4-methylphenyl)porphyrin

Downstream raw materials:

2,6,14-[tris(5-n-butyl-10,20-bis(4-methylphenyl)porphyrin-15-ylato)zinc(II)]triptycene

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