2,7-diphenyl-5H,6H,7H-imidazo[2,1-b]-1,4-thiazolium-3-thiolate

Base Information

• Chemical Name: 2,7-diphenyl-5H,6H,7H-imidazo[2,1-b]-1,4-thiazolium-3-thiolate
• CAS No.: 1146939-48-1
• Molecular Formula: C₁₇H₁₄N₂S₂
• Molecular Weight: 310.444
• Mol file: 1146939-48-1.mol

Synonyms:2,7-diphenyl-5H,6H,7H-imidazo[2,1-b]-1,4-thiazolium-3-thiolate

Chemical Property of 2,7-diphenyl-5H,6H,7H-imidazo[2,1-b]-1,4-thiazolium-3-thiolate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,7-diphenyl-5H,6H,7H-imidazo[2,1-b]-1,4-thiazolium-3-thiolate

There total 3 articles about 2,7-diphenyl-5H,6H,7H-imidazo[2,1-b]-1,4-thiazolium-3-thiolate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

2,7-Diphenyl-5H,6H,7H-imidazole[2,1-b]-1,4-thiazolium-3-thiolate (150928-59-9) + p-nitrophenyl isothiocyanate (2131-61-5) → 2,7-diphenyl-5H,6H,7H-imidazo[2,1-b]-1,4-thiazolium-3-thiolate (1146939-48-1) + 3,8-diphenyl-1-(4-nitrophenyl)-4-oxoimidazo[1,2-a]pyrimidin-5-ylium-2-olate (1146939-54-9) + 3,8-diphenyl-1-(4-nitrophenyl)-4-oxoimidazo[1,2-a]pyrimidin-5-ylium-2-thiolate (1146939-53-8)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1021/jo900028c

Reference yield: 73.0%

phenyl isothiocyanate (103-72-0) + 2,7-Diphenyl-5H,6H,7H-imidazole[2,1-b]-1,4-thiazolium-3-thiolate (150928-59-9) → 2,7-diphenyl-5H,6H,7H-imidazo[2,1-b]-1,4-thiazolium-3-thiolate (1146939-48-1) + 1,3,8-triphenyl-4-oxoimidazo[1,2-a]pyrimidin-5-ylium-2-thiolate (1146939-49-2) + 1,3,8-triphenyl-4-oxoimidazo[1,2-a]pyrimidin-5-ylium-2-olate (1146939-50-5)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1021/jo900028c

Reference yield: 9.0%

4-Methoxyphenyl isothiocyanate (2284-20-0) + 2,7-Diphenyl-5H,6H,7H-imidazole[2,1-b]-1,4-thiazolium-3-thiolate (150928-59-9) → 2,7-diphenyl-5H,6H,7H-imidazo[2,1-b]-1,4-thiazolium-3-thiolate (1146939-48-1) + 3,8-diphenyl-1-(4-methoxyphenyl)-4-oxoimidazo[1,2-a]pyrimidin-5-ylium-2-thiolate (1146939-51-6) + 3,8-diphenyl-1-(4-methoxyphenyl)-4-oxoimidazo[1,2-a]pyrimidin-5-ylium-2-olate (1146939-52-7)

Guidance literature:

In dichloromethane; at 20 ℃;

DOI:10.1021/jo900028c

upstream raw materials:

phenyl isothiocyanate

2,7-Diphenyl-5H,6H,7H-imidazole[2,1-b]-1,4-thiazolium-3-thiolate

4-Methoxyphenyl isothiocyanate

p-nitrophenyl isothiocyanate