C₂₆H₂₅F₃N₂O₃

Base Information

Chemical Name:C₂₆H₂₅F₃N₂O₃
CAS No.:1200496-82-7
Molecular Formula:C₂₆H₂₅F₃N₂O₃
Molecular Weight:470.491
Hs Code.:

C<sub>26</sub>H<sub>25</sub>F<sub>3</sub>N<sub>2</sub>O<sub>3</sub>

Synonyms:C₂₆H₂₅F₃N₂O₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₆H₂₅F₃N₂O₃

Chemical Property:

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Technology Process of C₂₆H₂₅F₃N₂O₃

There total 7 articles about C₂₆H₂₅F₃N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1200496-80-5
C₁₈H₁₉F₃N₂O

: 501-53-1,94274-21-2
benzyl chloroformate

: 1200496-82-7
C₂₆H₂₅F₃N₂O₃

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; for 1h; Inert atmosphere; Cooling with ice;

Reference yield:

: 434-45-7
2,2,2-Trifluoroacetophenone

: 1200496-82-7
C₂₆H₂₅F₃N₂O₃

Guidance literature:: Multi-step reaction with 7 steps

1.1: nitric acid; sulfuric acid / 2 h / -25 - -15 °C

2.1: hydrogenchloride; water; iron / methanol / Cooling with ice

2.2: Cooling with ice

3.1: ethyl acetate / 2 h / 20 °C

4.1: pyridinium p-toluenesulfonate / toluene / 10 h / 130 °C / Dean-Stark apparatus

5.1: tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

6.1: hydrogenchloride; water / ethanol / 5 h / 90 °C

7.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

With hydrogenchloride; sulfuric acid; water; nitric acid; iron; N-ethyl-N,N-diisopropylamine; pyridinium p-toluenesulfonate; In tetrahydrofuran; methanol; ethanol; dichloromethane; ethyl acetate; toluene;

Reference yield:

: 23516-80-5
3-amino-α,α,α-trifluoroacetophenone

: 1200496-82-7
C₂₆H₂₅F₃N₂O₃

Guidance literature:: Multi-step reaction with 5 steps

1: ethyl acetate / 2 h / 20 °C

2: pyridinium p-toluenesulfonate / toluene / 10 h / 130 °C / Dean-Stark apparatus

3: tetrahydrofuran / 1.5 h / -78 °C / Inert atmosphere

4: hydrogenchloride; water / ethanol / 5 h / 90 °C

5: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / Inert atmosphere; Cooling with ice

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; pyridinium p-toluenesulfonate; In tetrahydrofuran; ethanol; dichloromethane; ethyl acetate; toluene;