benzyl 2-(6-(methylamino)pyridin-2-yl)ethylcarbamate

Base Information

Chemical Name:benzyl 2-(6-(methylamino)pyridin-2-yl)ethylcarbamate
CAS No.:1220596-13-3
Molecular Formula:C₁₆H₁₉N₃O₂
Molecular Weight:285.346
Hs Code.:

Synonyms:benzyl 2-(6-(methylamino)pyridin-2-yl)ethylcarbamate

Suppliers and Price of benzyl 2-(6-(methylamino)pyridin-2-yl)ethylcarbamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 2-(6-(methylamino)pyridin-2-yl)ethylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 2-(6-(methylamino)pyridin-2-yl)ethylcarbamate

There total 1 articles about benzyl 2-(6-(methylamino)pyridin-2-yl)ethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 84713-20-2
benzyl N-vinylcarbamate

: 89026-79-9
2-bromo-6-(methylamino)pyridine

: 1220596-13-3
benzyl 2-(6-(methylamino)pyridin-2-yl)ethylcarbamate

Guidance literature:: benzyl N-vinylcarbamate; With 9-bora-bicyclo[3.3.1]nonane; In tetrahydrofuran; at 0 - 20 ℃; for 16h; Inert atmosphere;

With sodium hydroxide; In tetrahydrofuran; water; at 0 - 20 ℃; for 2h; Inert atmosphere;

2-bromo-6-(methylamino)pyridine; With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In tetrahydrofuran; water; at 65 ℃; for 24h; Inert atmosphere;
DOI:10.1016/j.tet.2010.01.025

Reference yield:

: 1220596-13-3
benzyl 2-(6-(methylamino)pyridin-2-yl)ethylcarbamate

: 1227094-87-2
1-(3,4-dichlorobenzyl)-3-(2-(6-(methylamino)pyridin-2-yl)ethyl)urea

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / ethanol / 24 h / 20 °C / 760.05 Torr

2: dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere

With hydrogen; palladium 10% on activated carbon; In ethanol; dichloromethane;