(S)-[2-acetyl-9-(p-toluenesulfonyl)-2,3,4,9-tetrahydro-1H-β-carbolin-1-yl]acetaldehyde

Base Information

Chemical Name:(S)-[2-acetyl-9-(p-toluenesulfonyl)-2,3,4,9-tetrahydro-1H-β-carbolin-1-yl]acetaldehyde
CAS No.:633307-67-2
Molecular Formula:C₂₂H₂₂N₂O₄S
Molecular Weight:410.494
Hs Code.:

Synonyms:(S)-[2-acetyl-9-(p-toluenesulfonyl)-2,3,4,9-tetrahydro-1H-β-carbolin-1-yl]acetaldehyde

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-[2-acetyl-9-(p-toluenesulfonyl)-2,3,4,9-tetrahydro-1H-β-carbolin-1-yl]acetaldehyde

Chemical Property:

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Technology Process of (S)-[2-acetyl-9-(p-toluenesulfonyl)-2,3,4,9-tetrahydro-1H-β-carbolin-1-yl]acetaldehyde

There total 4 articles about (S)-[2-acetyl-9-(p-toluenesulfonyl)-2,3,4,9-tetrahydro-1H-β-carbolin-1-yl]acetaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-[(S)-1-(2,3-Dihydroxy-propyl)-9-(toluene-4-sulfonyl)-1,3,4,9-tetrahydro-β-carbolin-2-yl]-ethanone

: 633307-67-2
(S)-[2-acetyl-9-(p-toluenesulfonyl)-2,3,4,9-tetrahydro-1H-β-carbolin-1-yl]acetaldehyde

Guidance literature:: With sodium periodate; In water; acetone; for 10h;
DOI:10.1021/ol030103x

Reference yield:

: 181218-86-0
(S)-1-allyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole

: 633307-67-2
(S)-[2-acetyl-9-(p-toluenesulfonyl)-2,3,4,9-tetrahydro-1H-β-carbolin-1-yl]acetaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / triethylamine / CH₂Cl₂ / 2 h / 20 °C

2: 45.3 percent / NaH / tetrahydrofuran / 23 h / 0 - 20 °C

3: OsO₄; N-methylmorpholine N-oxide / acetone; H₂O / 8.5 h / 20 °C

4: 216.8 mg / NaIO₄ / acetone; H₂O / 10 h

With sodium periodate; osmium(VIII) oxide; sodium hydride; 4-methylmorpholine N-oxide; triethylamine; In tetrahydrofuran; dichloromethane; water; acetone;
DOI:10.1021/ol030103x

Reference yield:

: 633307-65-0
(S)-1-(1-allyl-1,3,4,9-tetrahydro-β-carbolin-2-yl)ethanone

: 633307-67-2
(S)-[2-acetyl-9-(p-toluenesulfonyl)-2,3,4,9-tetrahydro-1H-β-carbolin-1-yl]acetaldehyde

Guidance literature:: Multi-step reaction with 3 steps

1: 45.3 percent / NaH / tetrahydrofuran / 23 h / 0 - 20 °C

2: OsO₄; N-methylmorpholine N-oxide / acetone; H₂O / 8.5 h / 20 °C

3: 216.8 mg / NaIO₄ / acetone; H₂O / 10 h

With sodium periodate; osmium(VIII) oxide; sodium hydride; 4-methylmorpholine N-oxide; In tetrahydrofuran; water; acetone;
DOI:10.1021/ol030103x