(R)-2-(1-cyclohexylidene-4-methoxybutan-2-yl)-N-methoxy-4-(trifluoromethyl)benzamide

Base Information

Chemical Name:(R)-2-(1-cyclohexylidene-4-methoxybutan-2-yl)-N-methoxy-4-(trifluoromethyl)benzamide
CAS No.:1417712-59-4
Molecular Formula:C₂₀H₂₆F₃NO₃
Molecular Weight:385.427
Hs Code.:

Synonyms:(R)-2-(1-cyclohexylidene-4-methoxybutan-2-yl)-N-methoxy-4-(trifluoromethyl)benzamide

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Chemical Property of (R)-2-(1-cyclohexylidene-4-methoxybutan-2-yl)-N-methoxy-4-(trifluoromethyl)benzamide

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Technology Process of (R)-2-(1-cyclohexylidene-4-methoxybutan-2-yl)-N-methoxy-4-(trifluoromethyl)benzamide

There total 2 articles about (R)-2-(1-cyclohexylidene-4-methoxybutan-2-yl)-N-methoxy-4-(trifluoromethyl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1328746-00-4
N-methoxy-4-(trifluoromethyl)benzamide

: 1417712-48-1
C₁₁H₁₈O

: 1417712-59-4
(R)-2-(1-cyclohexylidene-4-methoxybutan-2-yl)-N-methoxy-4-(trifluoromethyl)benzamide

Guidance literature:: N-methoxy-4-(trifluoromethyl)benzamide; With (+)-bis(η²-ethylene)[η⁵-(1R,3R)-4-(4-bromophenyl)-3-(methoxycarbonyl)-1-(4-fluorophenyl)-1,2,3,4-tetrahydrocyclopenta[c]pyridinyl]rhodium(I); dibenzoyl peroxide; In dichloromethane; 2,2,2-trifluoroethanol; at 20 ℃; for 0.166667h;

C₁₁H₁₈O; In dichloromethane; 2,2,2-trifluoroethanol; at -20 ℃; for 18h; enantioselective reaction;
DOI:10.1002/anie.201611981

Reference yield:

: 1328746-00-4
N-methoxy-4-(trifluoromethyl)benzamide

: 1417712-48-1
C₁₁H₁₈O

: 1417712-59-4
(R)-2-(1-cyclohexylidene-4-methoxybutan-2-yl)-N-methoxy-4-(trifluoromethyl)benzamide

: (S)-2-(1-cyclohexylidene-4-methoxybutan-2-yl)-N-methoxy-4-(trifluoromethyl)benzamide

Guidance literature:: N-methoxy-4-(trifluoromethyl)benzamide; With C₄₉H₆₇O₂RhSi₂; dibenzoyl peroxide; In dichloromethane; at 23 ℃; for 0.25h; Inert atmosphere;

C₁₁H₁₈O; In dichloromethane; at -20 ℃; for 18h; Overall yield = 91 %; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja311956k