2-methylcyclohexa-1,4-dien-3-ylphosphonous acid-borane bis(N,N-diethylamide)

Base Information

Chemical Name:2-methylcyclohexa-1,4-dien-3-ylphosphonous acid-borane bis(N,N-diethylamide)
CAS No.:1449303-22-3
Molecular Formula:C₁₅H₃₂BN₂P
Molecular Weight:282.217
Hs Code.:

Synonyms:2-methylcyclohexa-1,4-dien-3-ylphosphonous acid-borane bis(N,N-diethylamide)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-methylcyclohexa-1,4-dien-3-ylphosphonous acid-borane bis(N,N-diethylamide)

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Technology Process of 2-methylcyclohexa-1,4-dien-3-ylphosphonous acid-borane bis(N,N-diethylamide)

There total 3 articles about 2-methylcyclohexa-1,4-dien-3-ylphosphonous acid-borane bis(N,N-diethylamide) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1449303-00-7
o-tolylphosphonous acid-borane bis(N,N-diethylamide)

: 1449303-22-3
2-methylcyclohexa-1,4-dien-3-ylphosphonous acid-borane bis(N,N-diethylamide)

Guidance literature:: With ammonia; sodium; In tetrahydrofuran; at -78 ℃; for 0.0833333h; Inert atmosphere; Schlenk technique;
DOI:10.1002/ejoc.201300344

Reference yield:

: 113544-73-3
N,N,N',N'-tetraethyl-P-(2-methylphenyl)phosphonous diamide

: 1449303-22-3
2-methylcyclohexa-1,4-dien-3-ylphosphonous acid-borane bis(N,N-diethylamide)

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

2: ammonia; sodium / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere; Schlenk technique

With ammonia; sodium; In tetrahydrofuran; diethyl ether; 2: |Birch Reduction;
DOI:10.1002/ejoc.201300344

Reference yield:

: 685-83-6
bis(diethylamino)chlorophosphine

: 1449303-22-3
2-methylcyclohexa-1,4-dien-3-ylphosphonous acid-borane bis(N,N-diethylamide)

Guidance literature:: Multi-step reaction with 3 steps

1: magnesium / diethyl ether; tetrahydrofuran / 2 h / 0 °C / Inert atmosphere; Schlenk technique

2: diethyl ether; tetrahydrofuran / 20 °C / Inert atmosphere; Schlenk technique

3: ammonia; sodium / tetrahydrofuran / 0.08 h / -78 °C / Inert atmosphere; Schlenk technique

With ammonia; sodium; magnesium; In tetrahydrofuran; diethyl ether; 3: |Birch Reduction;
DOI:10.1002/ejoc.201300344