α-(3,5-Dimethoxy-phenyl)-heneicosanol

Base Information

• Chemical Name: α-(3,5-Dimethoxy-phenyl)-heneicosanol
• CAS No.: 96377-33-2
• Molecular Formula: C₂₉H₅₂O₃
• Molecular Weight: 448.73
• Mol file: 96377-33-2.mol

Synonyms:α-(3,5-Dimethoxy-phenyl)-heneicosanol

Chemical Property of α-(3,5-Dimethoxy-phenyl)-heneicosanol

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of α-(3,5-Dimethoxy-phenyl)-heneicosanol

There total 1 articles about α-(3,5-Dimethoxy-phenyl)-heneicosanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Bromoeicosane (4276-49-7) + 3,5-dimethoxybenzaldehdye (7311-34-4) → α-(3,5-Dimethoxy-phenyl)-heneicosanol (96377-33-2)

Guidance literature:

Multistep reaction; (i) MeI, Mg, Et₂O, (ii) /BRN= 2042374/;

DOI:10.1021/jo01025a046

Reference yield:

α-(3,5-Dimethoxy-phenyl)-heneicosanol (96377-33-2) → 1-heneicosyl-3,5-dimethoxybenzene (96377-24-1)

Guidance literature:

With sulfuric acid; hydrogen; palladium on activated charcoal; In ethyl acetate; at 55 ℃;

DOI:10.1021/jo01025a046

Reference yield:

α-(3,5-Dimethoxy-phenyl)-heneicosanol (96377-33-2) → 1,3-dihydroxy-5-heneicosylbenzene (70110-59-7)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂, H₂SO₄ / Pd-C / ethyl acetate / 55 °C

2: Py*HCl / Heating

With sulfuric acid; hydrogen; pyridine hydrochloride; palladium on activated charcoal; In ethyl acetate;

DOI:10.1021/jo01025a046

upstream raw materials:

1-Bromoeicosane

3,5-dimethoxybenzaldehdye

Downstream raw materials:

1-heneicosyl-3,5-dimethoxybenzene

1,3-dihydroxy-5-heneicosylbenzene

5-Heneicosyl-resorcin-diacetat