3,5-dihydroxyhomophthalic acid

Base Information

• Chemical Name: 3,5-dihydroxyhomophthalic acid
• CAS No.: 60336-51-8
• Molecular Formula: C₉H₈O₆
• Molecular Weight: 212.159

Synonyms:3,5-dihydroxyhomophthalic acid

Chemical Property of 3,5-dihydroxyhomophthalic acid

Chemical Property:

Purity/Quality:

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Technology Process of 3,5-dihydroxyhomophthalic acid

There total 2 articles about 3,5-dihydroxyhomophthalic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

7-tert-Butoxycarbonylmethyl-9-oxo-1,4-dioxa-spiro[4.5]dec-7-ene-8-carboxylic acid tert-butyl ester (99392-82-2) → 3,5-dihydroxyhomophthalic acid (60336-51-8)

Guidance literature:

With hydrogen iodide; for 3h; Heating;

Reference yield:

→ 3,5-dihydroxyhomophthalic acid (60336-51-8)

Guidance literature:

Orcintricarbonsaeure-triethylester, wss. KOH, 125grad;

Reference yield: 100.0%

diazomethane (186581-53-3,908094-01-9,334-88-3) + 3,5-dihydroxyhomophthalic acid (60336-51-8) → methyl <3,5-dihydroxy-2-(methoxycarbonyl)phenyl>acetate (6110-30-1)

Guidance literature:

In diethyl ether;

upstream raw materials:

7-tert-Butoxycarbonylmethyl-9-oxo-1,4-dioxa-spiro[4.5]dec-7-ene-8-carboxylic acid tert-butyl ester

Downstream raw materials:

methyl <3,5-dihydroxy-2-(methoxycarbonyl)phenyl>acetate

Methyl-6-(carbomethoxymethyl)-3-methyl-β-resorcylat

Methyl-6-(carbomethoxymethyl)-5-formyl-β-resorcylat

Methyl-6-(carbomethoxymethyl)-3-formyl-β-resorcylat

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