13-[(2'R,4'S,5'R)-3-t-butoxycarbonyl-2'-(1'-naphthyl)-4-phenyl-1,3'-oxazolidine-5'-carbonyl]-7,10-(di-3,5-dinitrobenzoyl)-10-deacetylbaccatin III

Base Information

• Chemical Name: 13-[(2'R,4'S,5'R)-3-t-butoxycarbonyl-2'-(1'-naphthyl)-4-phenyl-1,3'-oxazolidine-5'-carbonyl]-7,10-(di-3,5-dinitrobenzoyl)-10-deacetylbaccatin III
• CAS No.: 1033962-62-7
• Molecular Formula: C₆₈H₆₃N₅O₂₄
• Molecular Weight: 1334.27

Synonyms:13-[(2'R,4'S,5'R)-3-t-butoxycarbonyl-2'-(1'-naphthyl)-4-phenyl-1,3'-oxazolidine-5'-carbonyl]-7,10-(di-3,5-dinitrobenzoyl)-10-deacetylbaccatin III

Chemical Property of 13-[(2'R,4'S,5'R)-3-t-butoxycarbonyl-2'-(1'-naphthyl)-4-phenyl-1,3'-oxazolidine-5'-carbonyl]-7,10-(di-3,5-dinitrobenzoyl)-10-deacetylbaccatin III

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Technology Process of 13-[(2'R,4'S,5'R)-3-t-butoxycarbonyl-2'-(1'-naphthyl)-4-phenyl-1,3'-oxazolidine-5'-carbonyl]-7,10-(di-3,5-dinitrobenzoyl)-10-deacetylbaccatin III

There total 1 articles about 13-[(2'R,4'S,5'R)-3-t-butoxycarbonyl-2'-(1'-naphthyl)-4-phenyl-1,3'-oxazolidine-5'-carbonyl]-7,10-(di-3,5-dinitrobenzoyl)-10-deacetylbaccatin III which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

7,10-(di-3',5'-dinitrobenzoyl)-10-deacetylbaccatin III (1033517-17-7) + (2R,4S,5R)-2-(1'-naphthyl)-3-t-butoxycarbonyl-4-phenyl-1,3-oxazolidine-5-carboxylic acid (1033962-60-5) → 13-[(2'R,4'S,5'R)-3-t-butoxycarbonyl-2'-(1'-naphthyl)-4-phenyl-1,3'-oxazolidine-5'-carbonyl]-7,10-(di-3,5-dinitrobenzoyl)-10-deacetylbaccatin III (1033962-62-7)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In ethyl acetate; at 25 ℃; for 2h;

Reference yield: 91.0%

13-[(2'R,4'S,5'R)-3-t-butoxycarbonyl-2'-(1'-naphthyl)-4-phenyl-1,3'-oxazolidine-5'-carbonyl]-7,10-(di-3,5-dinitrobenzoyl)-10-deacetylbaccatin III (1033962-62-7) → 13-[(2'R,3'S)-3'-t-butoxycarbonylamino-3'-phenyl-2'-hydroxypropinonyl]-7,10-(di-3'',5''-dinitrobenzoyl)-10-deacetylbaccatin III (1033517-38-2)

Guidance literature:

With methanol; toluene-4-sulfonic acid; In chloroform; at 20 ℃; for 3h;

upstream raw materials:

7,10-(di-3',5'-dinitrobenzoyl)-10-deacetylbaccatin III

(2R,4S,5R)-2-(1'-naphthyl)-3-t-butoxycarbonyl-4-phenyl-1,3-oxazolidine-5-carboxylic acid

Downstream raw materials:

13-[(2'R,3'S)-3'-t-butoxycarbonylamino-3'-phenyl-2'-hydroxypropinonyl]-7,10-(di-3'',5''-dinitrobenzoyl)-10-deacetylbaccatin III

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